Helium Purification via PSA and Membrane Separation

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Solution Overview

Problem

Existing methods lack an efficient solution for purifying a stream with a high helium concentration and do not effectively optimize helium purification in the presence of a second stream with lower helium content.

Innovation Solution

The method involves combining a feed stream with a second stream, processing it through a Pressure Swing Adsorption (PSA) device, and then using membrane separation to produce a high-purity helium stream, with optional catalytic oxidation units to enhance the process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional purification methods are used on high helium concentration streams, then purification is achieved, but the process is inefficient and cannot optimize purification when a second stream with lower helium content is present

Engineering Contradiction:
Improvepurification efficiencyVSAvoidprocess complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent combines two separate feed streams with different helium concentrations into a single combined feed stream that is processed together through the PSA unit, thereby optimizing the use of purification capacity and improving overall productivity

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The PSA device is designed to handle multiple feed streams with varying helium concentrations simultaneously, making it a multi-functional unit that can optimize purification for both high-concentration and low-concentration streams in a single operation

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Manufacturing precision

If a single PSA unit processes mixed streams, then purification is achieved, but achieving very high purity (>99.99%) requires additional separation stages

Engineering Contradiction:
Improvehelium purityVSAvoidnumber of separation stages
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent divides the purification process into two distinct PSA units with different functions: the first unit handles bulk purification and produces intermediate purity helium, while the second unit performs final polishing to achieve very high purity (>99.99%), with each unit optimized for its specific purification stage

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The first PSA unit acts as an intermediary stage that pre-purifies the helium stream before it enters the second PSA unit, reducing the burden on the final purification stage and enabling high purity output without requiring a single overly complex unit

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively purifies helium to a high quality, even when starting with a stream of significant helium content, and can optimize the purification process in the presence of a second stream with lower helium content, achieving high-purity helium production.

Implementation Method 1

introducing the combined feed stream into a pressure swing adsorption device, thereby producing a high purity product gas stream

Methodology Applied
Scientific EffectPressure Swing Adsorption: Pressure Swing Adsorption

Implementation Method 2

introducing the off-gas stream into a membrane separation device, thereby producing a gas stream lean in product gas and a permeate stream

Methodology Applied
Scientific EffectMembrane separation: Semipermeable Membrane

Data Source

PatentUS20240228285A9Process for producing very high purity helium or hydrogen
Publication Date: 2024.07.11 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • US20240228285A9 patent drawing
  • US20240228285A9 patent drawing
  • US20240228285A9 patent drawing

AI summary

A method of purifying a gas composed of a product gas and one or more impurity gases including combining a feed stream with a second stream thereby forming a combined feed stream, introducing the combined feed stream into a pressure swing adsorption device, thereby producing a high purity product gas stream and an off-gas stream, and introducing the off-gas stream into a membrane separation device, thereby producing a gas stream lean in product gas and a permeate stream.