Heterocyclic Electrolyte for Lithium-Sulfur Cycle Life Stability

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Solution Overview

Problem

Existing lithium-sulfur batteries face issues with deteriorated lifetime characteristics and lithium cycle efficiency due to the use of ether-based solvents, which lead to polysulfide leaching, dendrite growth, and increased viscosity during charging/discharging, limiting their application in high-energy density requirements for electric vehicles and energy storage systems.

Innovation Solution

An electrolyte solution for lithium-sulfur batteries comprising a first solvent with heterocyclic compounds containing double bonds and oxygen/sulfur atoms, a second solvent with ether-based, ester-based, or carbonate-based compounds, lithium salts, lithium nitrate, and borate-based lithium salts, forming a protective film to suppress polysulfide leaching and enhance ion conductivity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If ether-based solvent is used to improve sulfur reactivity, then lithium polysulfide dissolution is enhanced, but lifetime characteristics deteriorate due to polysulfide leaching and dendrite growth

Engineering Contradiction:
Improvesulfur reactivityVSAvoidlifetime characteristics
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The patent introduces a novel ether-based solvent with specific molecular structure (cyclic ether with oxygen atom in the ring) as an intermediary substance. This solvent mediates between sulfur polysulfides and lithium ions, enabling effective dissolution and reaction while the cyclic structure provides resistance to polysulfide leaching, thus resolving the contradiction between reactivity enhancement and lifetime deterioration

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent changes the chemical parameters of the ether-based solvent by specifying particular cyclic ether structures with defined molecular weights and ring sizes. This parameter optimization allows the solvent to maintain high polysulfide solubility while the cyclic structure prevents excessive polysulfide extraction, thereby improving both reactivity and lifetime characteristics simultaneously

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If electrolyte solution content is decreased to achieve high energy density, then energy storage capacity increases, but viscosity increases rapidly during charging/discharging causing overvoltage

Engineering Contradiction:
Improveenergy densityVSAvoidviscosity
Core Design Contradiction:
Quantity of substanceVSStress or pressure

Solution Approach 1:

The patent optimizes the molecular weight and structural parameters of the cyclic ether solvent to achieve the desired balance. By selecting specific cyclic ether compounds with appropriate molecular weights and ring structures, the electrolyte maintains low viscosity even at reduced concentrations, preventing overvoltage while achieving high energy density

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite electrolyte system by combining the novel cyclic ether-based solvent with lithium salt and other additives. This composite formulation ensures that the electrolyte maintains optimal conductivity and low viscosity characteristics even when the overall electrolyte content is reduced for high energy density applications

Inventive Principle:
Principle #40Composite materials

3Quantity of substance

If conventional ether-based solvent is used, then lithium polysulfide solubility is high, but decomposition occurs leading to by-product deposition

Engineering Contradiction:
Improvelithium polysulfide solubilityVSAvoiddecomposition by-products
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The patent employs a specifically designed cyclic ether solvent that acts as a sacrificial protective medium. The solvent preferentially reacts with and stabilizes lithium polysulfides through coordination, preventing their decomposition into harmful by-products. The solvent molecules form stable complexes with polysulfides, effectively protecting them from degradation while maintaining high solubility

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution improves the lifetime characteristics and lithium cycle efficiency of lithium-sulfur batteries by reducing polysulfide leaching and dendrite formation, maintaining stable conductivity, and extending cycle life.

Implementation Method 1

incorporating a first solvent comprising a heterocyclic compound containing one or more double bonds and at the same time, containing any one of an oxygen atom and a sulfur atom... forming a protective film to suppress polysulfide leaching and enhance ion conductivity

Methodology Applied
Scientific EffectFilm formation: Deposition (physical)

Implementation Method 2

The lithium cation produced by the oxidation reaction of lithium is transferred to the positive electrode through the electrolyte

Methodology Applied
Scientific EffectIonic conduction: Conduction (electrical)

Implementation Method 3

lithium salt, wherein the lithium salt is at least one selected from the group consisting of LiCl, LiBr, LiI, LiClO4, LiPF6, LiCF3SO3, LiCF3CO2, LiAsF6, LiSbF6, LiAlCl4, CH3SO3Li, CF3SO3Li, (C2F5SO2)2NLi, (SO2F)2NLi, (CF3SO2)3CLi, and lithium lower aliphatic carboxylate having 4 or less carbon atoms

Methodology Applied
Scientific EffectDissociation: Electrolyte

Data Source

PatentEP4152466B1Electrolyte for lithium-sulfur battery, and lithium-sulfur battery comprising same
Publication Date: 2025.07.23 LG ENERGY SOLUTION LTD
  • EP4152466B1 patent drawingFigure 1
  • EP4152466B1 patent drawingFigure 2

AI summary

The present invention relates to an electrolyte solution for a lithium-sulfur battery comprising a first solvent comprising a heterocyclic compound containing one or more double bonds and at the same time, containing any one of an oxygen atom and a sulfur atom; a second solvent comprising at least one of an ether-based compound, an ester-based compound, an amide-based compound, and a carbonate-based compound; lithium salt; lithium nitrate; and borate-based lithium salt, and a lithium-sulfur battery comprising the same.