Hexagonal Ferrite Magnetic Powder Manufacturing

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Solution Overview

Problem

Existing methods for manufacturing hexagonal ferrite magnetic powders struggle to achieve ultra-high-density recording due to broad particle size distributions, leading to noise and demagnetization issues, especially at recording densities above 1 Gbpsi.

Innovation Solution

A method involving the glass crystallization of a starting material mixture containing hexagonal ferrite and glass-forming components, with controlled carbon content (0.3 to 2.0 weight percent) and heat treatment within the 580 to 700°C temperature range to achieve a sharp particle size distribution, optimizing the reaction rate and particle growth.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional glass crystallization methods are used to manufacture hexagonal ferrite magnetic powder, then the manufacturing process is simple and cost-effective, but the particle size distribution is broad leading to noise and demagnetization issues

Engineering Contradiction:
Improveparticle size distributionVSAvoidmanufacturing process complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent applies parameter changes by precisely controlling the crystallization temperature (580-700°C) and carbon content (0.3-2.0 weight percent) during the glass crystallization process. These parameter optimizations transform the conventional simple method into a controlled process that achieves sharp particle size distribution while maintaining manufacturing feasibility.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent incorporates preliminary action by adding carbon-containing compounds to the starting material mixture before crystallization. This preliminary introduction of carbon serves as a nucleation promoter that controls the crystallization kinetics, ensuring uniform particle formation and sharp size distribution from the outset of the manufacturing process.

Inventive Principle:
Principle #10Preliminary action

2Quantity of substance

If particle size is reduced for high-density recording, then recording density increases, but thermal fluctuation causes demagnetization in smaller particles

Engineering Contradiction:
Improverecording densityVSAvoidmagnetic stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent changes the physical parameters of the magnetic powder by achieving a sharp particle size distribution through controlled crystallization. This produces particles with uniform dimensions that optimize the balance between small size (for high density) and sufficient magnetic moment (for thermal stability), enabling recording densities above 1 Gbpsi while maintaining reliability.

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If broad particle size distribution is accepted for easier manufacturing, then manufacturing is simpler, but signal-to-noise ratio deteriorates

Engineering Contradiction:
Improveparticle size distribution sharpnessVSAvoidmanufacturing simplicity
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The patent optimizes manufacturing parameters by controlling crystallization temperature (580-700°C) and carbon content (0.3-2.0 weight percent). These parameter changes enable the conventional glass crystallization method to produce sharp particle size distributions, achieving high manufacturing precision without significantly increasing process complexity.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces hexagonal ferrite magnetic powders with a sharp particle size distribution, enhancing signal-to-noise ratio (SNR) and reducing demagnetization, enabling reliable ultra-high-density recording.

Implementation Method 1

heating the amorphous material to a temperature range of 580 to 700° C. and maintaining the amorphous material within the temperature range to precipitate hexagonal ferrite magnetic particles

Methodology Applied
Scientific EffectCrystallization: Crystallisation

Implementation Method 2

rapidly cooling the melt to obtain an amorphous material comprising 0.3 to 2.0 weight percent of carbon atoms

Methodology Applied
Scientific EffectRapid cooling: Cooling

Data Source

PatentUS8419966B2Method of manufacturing hexagonal ferrite magnetic powder, magnetic recording medium and method of manufacturing the same
Publication Date: 2013.04.16 FUJIFILM CORP
  • US8419966B2 patent drawing
  • US8419966B2 patent drawing

AI summary

An aspect of the present invention relates to a method of manufacturing a hexagonal ferrite magnetic powder comprising preparing a melt by melting a starting material mixture comprising a hexagonal ferrite-forming component and a glass-forming component; rapidly cooling the melt to obtain an amorphous material comprising 0.3 to 2.0 weight percent of carbon atoms; heating the amorphous material to a temperature range of 580 to 700° C. and maintaining the amorphous material within the temperature range to precipitate hexagonal ferrite magnetic particles; and collecting the hexagonal ferrite magnetic particles precipitated.