HFC-143 Refrigerant Composition for Low-GWP Stable Separation

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Solution Overview

Problem

Existing refrigerant compositions do not effectively utilize 1,1,2-trifluoroethane (HFC-143) and lack stable, low-global warming potential alternatives to conventional HFC refrigerants like HFC134a, R-410A, R-407C, or R-404A.

Innovation Solution

A novel refrigerant composition comprising 1,1,2-trifluoroethane (HFC-143) with up to 10% 1-chloro-1,2,2-trifluoroethane (HCFC-133) and 1-chloro-1,1,2-trifluoroethane (HCFC-133b), and up to 1% of additional compounds like 1,1,2-trifluoroethylene (HFC-1123), achieving a total composition of ≥99.5% HFC-143 and HCFC-133a, suitable for azeotropic distillation and use as a heat transfer medium.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If conventional HFC refrigerants like HFC134a, R-410A, R-407C, or R-404A are used, then refrigerant performance is maintained, but global warming potential is high

Engineering Contradiction:
Improveglobal warming potentialVSAvoidrefrigerant performance stability
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters by using HFC-143 as the base refrigerant and controlling the content of specific compounds (HCFC-133, HCFC-133b, HCFO-1131, and additional compounds) within defined ranges. This parameter change achieves low global warming potential while maintaining refrigerant performance through optimized compositional parameters.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite refrigerant mixture by combining HFC-143 with specific compounds (HCFC-133, HCFC-133b, HCFO-1131, and additional compounds from the selected list) in controlled proportions. This composite approach maintains refrigerant performance while reducing environmental harm through the synergistic effect of multiple components.

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If HFC-143 is used as a refrigerant, then low global warming potential is achieved, but separation difficulty increases due to similar boiling points with other fluorine-containing compounds

Engineering Contradiction:
Improveglobal warming potentialVSAvoidseparation process complexity
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

The patent addresses separation difficulty by precisely controlling the compositional parameters of the refrigerant mixture. By defining specific content ranges for compounds with similar boiling points, the patent enables effective separation through azeotropic distillation while maintaining the low global warming potential benefits of HFC-143.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses azeotropic distillation as an intermediary separation method to isolate HFC-143 from other fluorine-containing compounds. This intermediary technique leverages the formation of azeotropic mixtures to achieve separation based on boiling point similarities, making the separation process more manageable despite the close boiling points of the components.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If the refrigerant composition is highly purified to ≥99.5% HFC-143 and HCFC-133a, then separation efficiency improves, but manufacturing precision requirements increase

Engineering Contradiction:
Improveseparation efficiencyVSAvoidcomposition control precision
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent balances separation efficiency with manufacturing feasibility by establishing specific compositional parameters and content ranges for the refrigerant components. These parameter definitions enable high purity (≥99.5%) while providing practical guidance for manufacturing control, avoiding excessively tight tolerances that would be difficult to achieve.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent achieves high separation efficiency by concentrating on the removal of specific problematic compounds rather than attempting to remove all impurities equally. By focusing on the main interfering substances and setting appropriate removal thresholds, the patent achieves ≥99.5% purity with reasonable manufacturing precision requirements.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition provides a stable, low-global warming potential refrigerant with improved separation capabilities and can be used as a drop-in alternative to conventional HFC refrigerants, maintaining refrigerating machine performance with minimal equipment adjustments.

Implementation Method 1

achieving a total composition of ≥99.5% HFC-143 and HCFC-133a, suitable for azeotropic distillation

Methodology Applied
Scientific EffectAzeotropic distillation: Distillation

Data Source

PatentEP3940037B1Composition including 1,1,2-trifluoroethane (HFC-143)
Publication Date: 2025.12.03 DAIKIN INDUSTRIES LTD
  • EP3940037B1 patent drawingFigure 1

AI summary

A novel composition comprising HFC-143 is provided. This invention relates to a composition comprising a refrigerant, wherein the refrigerant comprises 1,1,2-trifluoroethane (HFC-143), and at least one compound selected from the group consisting of 1-chloro-1,2,2-trifluoroethane (HCFC-133), 1-chloro-1,1,2-trifluoroethane (HCFC-133b), and 1-chloro-2-fluoroethylene (HCFO-1131).