High Chain Length Inulin Purification for Thermal Stability

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current inulins used in food and cosmetic products face issues with processing properties such as viscosity, thermal stability, emulsifiability, and prebiotic effectiveness, and are contaminated with mono- and disaccharides, which interfere with processing and storage, leading to unwanted reactions and flavor changes.

Innovation Solution

A spray-dried inulin with a specific molecular weight range (83-103) and reduced content of mono- and disaccharides, produced through a process involving artichoke roots extraction and purification, offering improved stability, emulsifiability, and prebiotic properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If inulin is extracted from plant tissue using hot water, then inulin can be obtained for use in food products, but the extract contains mono- and disaccharides and fructooligosaccharides that interfere with further processing and storage

Engineering Contradiction:
Improveinulin contentVSAvoidmono- and disaccharides and fructooligosaccharides
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The patent applies extraction by selectively removing harmful components (mono- and disaccharides, fructooligosaccharides) from the inulin extract through purification steps including filtration, centrifugation, and chromatography, thereby obtaining high-purity inulin suitable for food applications

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes physical and chemical parameters during processing, including temperature control during extraction, pH adjustment, and molecular weight fractionation, to optimize inulin recovery while minimizing harmful by-products and improving processing properties

Inventive Principle:
Principle #35Parameter changes

2Reliability

If conventional inulin is used in food products, then it provides prebiotic effects and low energy value, but it has unsatisfactory processing properties such as viscosity, thermal stability, and emulsifiability

Engineering Contradiction:
Improveprebiotic effect and low energy valueVSAvoidviscosity and thermal stability
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent segments inulin into different molecular weight fractions, selecting and purifying the high molecular weight fraction (DPw 83-103) that exhibits superior processing properties including better viscosity control, thermal stability, and emulsifiability while maintaining prebiotic effectiveness

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent produces a composite inulin product with controlled molecular weight distribution and reduced contaminant content, creating a material that combines the functional benefits of inulin (prebiotic effect, low energy value) with improved processing characteristics

Inventive Principle:
Principle #40Composite materials

3Ease of manufacture

If crude inulin is used in food products, then it is readily available from plant sources, but it causes unwanted browning reactions, off-flavors, and acrylamide formation during thermal processing

Engineering Contradiction:
Improveavailability from plant sourcesVSAvoidbrowning reactions and off-flavors
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent performs preliminary purification and molecular weight fractionation of inulin before use in food products, removing reducing sugars and fructooligosaccharides that cause Maillard reactions, thereby preventing browning, off-flavor formation, and acrylamide generation during subsequent thermal processing

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The inulin exhibits enhanced thermal stability, shear resistance, and prebiotic effects, reducing gas formation in the bowel and promoting bifidobacteria growth, while improving sensory and baking properties, and reducing unwanted by-products.

Implementation Method 1

The invention relates to an inulin which has an average degree of polymerization DPw, determined by GPC-RI-MALLS, of between 83 and 103, preferably between 84 and 100, more preferably between 83 and 98, even more preferably between 85 and 98, yet more preferably 85 and 95, still more preferably between 86 and 97 and most preferably between 86 and 94, characterized in that the inulin is spray dried.

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentEP2016104B1Inulin of very high chain length
Publication Date: 2010.12.22 BAYER CROPSCIENCE AG
  • EP2016104B1 patent drawingFigure 1
  • EP2016104B1 patent drawingFigure 2~3
  • EP2016104B1 patent drawingFigure 4~5

AI summary

The invention relates to a long-chain inulin and its preparation from artichoke roots, to its use in foodstuffs and cosmetic preparations and to foodstuffs and cosmetic preparations which comprise the long-chain inulin.