High-Fat Protein Emulsion Stability via Heat Stabilization

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Solution Overview

Problem

High-fat, high-energy liquid nutritional compositions face challenges with heat stability and emulsion reversal, particularly when enriched with minerals and vitamins, leading to sedimentation and microbiological instability, which limits their shelf-life and commercial viability.

Innovation Solution

A shelf-stable liquid aqueous nutritional composition incorporating non-micellar casein with a fat content of 30-50 g/100 ml, combined with a heat stabilization system using potassium citrate or potassium dihydrogen phosphate, and optional emulsifiers like phospholipids, to prevent sedimentation and maintain stability during sterilization.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If high-fat content (30-50 g/100 ml) is incorporated into liquid nutritional composition, then caloric density and energy content are improved, but heat stability and emulsion stability deteriorate, leading to sedimentation and emulsion reversal during sterilization

Engineering Contradiction:
Improvecaloric densityVSAvoidemulsion stability
Core Design Contradiction:
Use of energy by moving objectVSStability of the object's composition

Solution Approach 1:

The patent introduces a heat stabilisation system comprising potassium citrate or potassium dihydrogen phosphate as intermediary substances that mediate between the high-fat content and the emulsion stability. These stabilisers prevent direct interaction between fat and protein that would cause emulsion reversal, thereby maintaining emulsion stability even at 30-50 g/100 ml fat content during sterilization

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent changes the chemical composition parameters by incorporating specific heat stabilisers (potassium citrate or potassium dihydrogen phosphate) at controlled concentrations. This parameter change modifies the pH and ionic strength of the emulsion, preventing casein precipitation and emulsion reversal during heat treatment, thus enabling high-fat content while maintaining stability

Inventive Principle:
Principle #35Parameter changes

2Use of energy by moving object

If high-fat content is incorporated into liquid nutritional composition, then energy content is improved, but microbiological stability deteriorates, leading to spoilage and reduced shelf-life

Engineering Contradiction:
Improveenergy contentVSAvoidmicrobiological stability
Core Design Contradiction:
Use of energy by moving objectVSReliability

Solution Approach 1:

The patent applies preliminary heat treatment (sterilization) to the liquid nutritional composition before packaging. The heat stabilisation system is incorporated beforehand to ensure that when heat treatment is applied, the composition remains stable and does not undergo emulsion reversal or protein precipitation, thus achieving microbiological stability and extended shelf-life while maintaining high energy content

Inventive Principle:
Principle #10Preliminary action

3Quantity of substance

If minerals and vitamins are enriched in high-fat nutritional composition, then nutritional value is improved, but heat stability deteriorates, causing sedimentation and instability during sterilization

Engineering Contradiction:
Improvenutritional valueVSAvoidheat stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The heat stabilisation system (potassium citrate or potassium dihydrogen phosphate) acts as an intermediary that prevents direct interaction between minerals/vitamins and the emulsion components during heat treatment. This stabiliser system chelates metal ions and buffers pH changes, preventing precipitation and maintaining nutritional value while ensuring heat stability during sterilization

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition achieves long-term stability and microbiological safety, preventing sedimentation and emulsion reversal, ensuring a stable product suitable for malnourished individuals and those with compromised gastrointestinal tracts.

Implementation Method 1

comprising a heat stabilisation system

Methodology Applied
Scientific EffectHeat stabilisation:

Implementation Method 2

liquid aqueous nutritional composition

Methodology Applied
Scientific EffectEmulsion: Emulsion

Data Source

PatentEP2346356B2Liquid high-fat protein composition
Publication Date: 2019.08.07 NV NUTRICIA

AI summary

The invention concernsnutritional compositionsfor persons with a (partially) functional gastrointestinal tract, who are unwilling and/or unable to consume sufficient quantities of conventional food to meet their nutritional requirementssuch as malnourished persons or persons at risk of becoming malnourished, and in need of liquid oral nutrition.The shelf-stable liquid nutritional compositionscompriseat least non-micellar casein, a high amount of fat, and optionally a heat stabilisation system.