High-Pressure PSA Integration for Hydroprocessing Hydrogen Recovery

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Solution Overview

Problem

Current hydroprocessing units face inefficiencies in hydrogen recovery and utilization, leading to increased capital and operating expenses, particularly in complexes lacking integrated high-pressure pressure swing adsorption (PSA) units, which limits the overall economics and hydrogen balance.

Innovation Solution

Incorporating a PSA unit within the make-up gas compression system of hydroprocessing units at higher pressures (3447.4 kPa to 6894.8 kPa) and utilizing a chiller to reduce feed gas temperature, thereby enhancing hydrogen recovery and reducing equipment size and compression power.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If a conventional stand-alone PSA unit is used at low pressure (300-400 psig), then the PSA unit can operate with standard equipment, but hydrogen recovery is limited to 85-90% and additional booster compressors are required

Engineering Contradiction:
ImprovePSA unit operationVSAvoidhydrogen recovery
Core Design Contradiction:
Ease of manufactureVSLoss of substance

Solution Approach 1:

The patent applies parameter changes by operating the PSA unit at significantly higher pressure (500-1000 psig) compared to conventional low-pressure operation (300-400 psig). This pressure increase improves hydrogen recovery by 3-6 percentage points and eliminates the need for additional booster compressors, directly resolving the contradiction between ease of manufacture and hydrogen recovery loss

Inventive Principle:
Principle #35Parameter changes

2Loss of substance

If a PSA unit is integrated into the make-up gas compression system at high pressure, then hydrogen recovery increases by 3-6 percentage points, but equipment complexity and initial investment increase

Engineering Contradiction:
Improvehydrogen recoveryVSAvoidequipment count
Core Design Contradiction:
Loss of substanceVSDevice complexity

Solution Approach 1:

The patent merges the PSA unit with the existing make-up gas compression system, integrating hydrogen recovery functionality into the hydrocracker's compression infrastructure. This integration improves hydrogen recovery while minimizing additional equipment by utilizing the existing high-pressure environment and compression capabilities

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent extracts the need for separate booster compressors by taking out the compression function and incorporating it directly into the PSA unit operation at high pressure. This eliminates redundant equipment while maintaining improved hydrogen recovery

Inventive Principle:
Principle #2Taking out (Extraction)

3Device complexity

If PSA hydrogen product is produced at low pressure, then equipment requirements are simpler, but multiple stages of make-up gas compression are required to reach reaction system pressure

Engineering Contradiction:
Improvecompression stagesVSAvoidcompression power
Core Design Contradiction:
Device complexityVSUse of energy by moving object

Solution Approach 1:

The patent changes the pressure parameter of the PSA operation from conventional low pressure to high pressure (500-1000 psig), matching the hydrocracker operating pressure range. This eliminates the need for multiple compression stages and reduces compression power consumption while maintaining simpler equipment requirements

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach increases hydrogen recovery by 3 to 6 percentage points, reduces equipment count, and decreases costs by allowing smaller PSA units and lower compressor power consumption, providing a synergistic benefit that conventional stand-alone PSA units cannot achieve.

Implementation Method 1

a pressure swing adsorption (PSA) unit to derive pure hydrogen (99.9 mol%) that is used as make-up gas to the hydrocracking unit

Methodology Applied
Scientific EffectPressure swing adsorption: Pressure Swing Adsorption

Implementation Method 2

the compressed gas stream is sent to a pressure swing adsorption unit containing a plurality of beds with at least 5 pressure equalization steps to produce a hydrogen stream

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 3

utilizing a chiller to reduce feed gas temperature, thereby enhancing hydrogen recovery

Methodology Applied
Scientific EffectRefrigeration cooling: Cooling

Data Source

PatentEP3743372B1Integration of pressure swing adsorption and hydroprocessing for improved hydrogen utilization
Publication Date: 2023.10.11 UOP LLC
  • EP3743372B1 patent drawingFigure 1
  • EP3743372B1 patent drawingFigure 2
  • EP3743372B1 patent drawingFigure 3

AI summary

The invention provides a process for providing a hydrogen stream to a process utilizing hydrogen comprising obtaining a gas stream containing hydrogen and compressing the gas stream to a pressure of at least 600 psig, Then the compressed gas stream is sent to a pressure swing adsorption unit containing a plurality of beds with at least 5 pressure equalization steps to produce a hydrogen stream. The hydrogen stream can then be compressed and sent to a process utilizing hydrogen. The compressed gas stream may be chilled before entering the pressure swing adsorption unit.