Hydrothermal Liquefaction Electrolyzer for Biomass Deoxygenation

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Solution Overview

Problem

Conventional hydrothermal liquefaction processes face challenges due to the accumulation of oxygenated organic compounds in the aqueous phase, which reduces the calorific value of biofuel and decreases overall yield, requiring costly purification methods and specific equipment.

Innovation Solution

Combining hydrothermal liquefaction with electrolysis to deoxygenate organic molecules in the aqueous phase, converting them into hydrocarbon compounds, and recycling the treated phase to improve biomass treatment efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by stationary object

If the aqueous phase is recycled to initiate a new hydrothermal liquefaction cycle, then the process continuity is improved, but the rate of inorganics in the biomass / recycled water mixture increases

Engineering Contradiction:
Improveprocess continuityVSAvoidrate of inorganics
Core Design Contradiction:
Use of energy by stationary objectVSQuantity of substance

Solution Approach 1:

The patent extracts and removes inorganic compounds from the recycled aqueous phase through filtration or separation processes before reusing the water in subsequent hydrothermal liquefaction cycles. This maintains process continuity while preventing inorganic accumulation that would otherwise degrade reaction performance.

Inventive Principle:
Principle #2Taking out (Extraction)

2Manufacturing precision

If conventional hydrotreatment techniques are used to eliminate oxygenated compounds, then the purity of biofuel is improved, but specific equipment and high pressure hydrogen are required

Engineering Contradiction:
Improvepurity of biofuelVSAvoidspecific equipment
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent replaces complex mechanical hydrotreatment systems with a biochemical approach using enzymes or microorganisms that catalyze the removal of oxygenated compounds under milder conditions. This eliminates the need for high-pressure hydrogen equipment while achieving comparable purification results.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Reliability

If the presence of oxygenates is eliminated by conventional hydrotreatment, then the aging of oil is reduced, but the overall yield of biofuel generation decreases

Engineering Contradiction:
Improvestability of biofuelVSAvoidoverall yield of biofuel
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent modifies process parameters such as temperature, pH, or catalyst composition to enable selective removal of oxygenated compounds that cause aging, while preserving the hydrocarbon components that contribute to biofuel yield. This optimization maintains both stability and productivity.

Inventive Principle:
Principle #35Parameter changes

4Use of energy by moving object

If organic compounds are removed from the aqueous phase, then the calorific value of biofuel is improved, but the yield of oil production from biomass transformation decreases

Engineering Contradiction:
Improvecalorific value of biofuelVSAvoidyield of oil production
Core Design Contradiction:
Use of energy by moving objectVSProductivity

Solution Approach 1:

The patent applies localized treatment to specific portions of the aqueous phase or targets specific oxygenated compounds rather than removing all organic matter uniformly. This selective approach improves calorific value by eliminating problematic oxygenates while retaining beneficial organic compounds that contribute to oil yield.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enhances the overall efficiency of biomass treatment by reducing oxygen content, improving biofuel yield, and eliminating the need for external purification steps, while utilizing recycled hydrogen for hydro-deoxygenation.

Implementation Method 1

the electrolyzer makes it possible to deoxygenate the organic molecules present in the aqueous phase to form hydrocarbon compounds (hydrocarbons)

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Implementation Method 2

The hydrothermal liquefaction process is generally carried out in water, under pressure and at a temperature of the order of 280 to 350 °C

Methodology Applied
Scientific EffectHydrothermal liquefaction:

Data Source

PatentEP3286284B1Device and method for treating biomass
Publication Date: 2019.06.05 COMMISSARIAT A LENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES
  • EP3286284B1 patent drawingFigure 1~2

AI summary

The present invention relates to a device for treating biomass by hydrothermal liquefaction, which includes: a pump (2) for injecting a biomass fluid and water; a reactor (3) for hydrothermal liquefaction of the fluid, downstream from the injection pump (2); a separation unit (4), downstream from the hydrothermal liquefaction reactor (3), the separation unit (4) including an aqueous phase outlet and an organic phase outlet; an electrolyser (9), downstream from the aqueous phase outlet of the separation unit (4); and a connection linking the electrolyser (9) to the injection pump (2). The present invention also relates to the method for transforming biomass which implements said device.