Humic Substance Extraction from Landfill Leachate

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Solution Overview

Problem

Existing processes for treating sanitary landfill leachate do not effectively extract and purify humic substances, which are valuable for agriculture due to their soil conditioning and nutrient facilitation properties, despite their high concentration in landfill slurry.

Innovation Solution

A four-step process involving physical-chemical coagulation and flocculation, filtration through sand, microfiltration, and nanofiltration, followed by reverse osmosis and catalytic oxidation to concentrate humic substances and treat the effluent for reuse, utilizing FeCl3, anionic and cationic polymers, and ionic exchange resins.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If existing treatment processes are used for sanitary landfill leachate, then the treatment can be performed with simple equipment, but humic substances cannot be effectively extracted and purified

Engineering Contradiction:
Improveextraction and purification of humic substancesVSAvoidtreatment process complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The treatment process is divided into multiple sequential stages: coagulation-flocculation, sand filtration, microfiltration, nanofiltration, and reverse osmosis. Each stage targets specific contaminants and progressively concentrates humic substances, transforming a single complex extraction task into manageable sequential steps that achieve high purification precision.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent employs nested filtration systems where microfiltration membranes are combined with nanofiltration membranes, which are in turn combined with reverse osmosis membranes. This nested structure allows each filtration stage to build upon the previous one, with progressively smaller pore sizes and higher rejection rates, enabling effective humic substance extraction while organizing complex equipment in a hierarchical manner.

Inventive Principle:
Principle #7Nested doll (Nesting)

2Quantity of substance

If physical-chemical coagulation and flocculation is used to extract humic substances, then the concentration of humic substances increases, but the effluent requires further treatment to meet environmental regulations

Engineering Contradiction:
Improveconcentration of humic substancesVSAvoideffluent quality
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The coagulation-flocculation process selectively extracts and concentrates humic substances from the leachate by forming removable flocs. This separation allows the humic-rich concentrate to be harvested for agricultural use while the treated effluent proceeds to additional treatment stages to remove remaining contaminants before discharge or reuse.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

Coagulants and flocculants act as intermediary substances that bridge the gap between dissolved humic substances and removable particulate matter. These chemicals facilitate the aggregation of humic substances into flocs that can be easily separated, while subsequent treatment stages use additional intermediaries to address remaining effluent quality issues.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Object-affected harmful factors

If multiple filtration stages are implemented to purify effluent, then the effluent quality improves to meet regulations, but the process time and operational complexity increase

Engineering Contradiction:
Improveeffluent qualityVSAvoidprocess time
Core Design Contradiction:
Object-affected harmful factorsVSLoss of time

Solution Approach 1:

Coagulation and flocculation are performed as preliminary treatment stages to remove the bulk of suspended solids and concentrate humic substances before the effluent enters the filtration system. This preliminary action reduces the contaminant load entering subsequent filtration stages, allowing them to operate more efficiently and reduce overall process time while maintaining high effluent quality.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent employs a series of filtration stages with progressively changing parameters - pore size decreases from microfiltration to nanofiltration to reverse osmosis, while pressure and rejection rates increase. This systematic parameter progression optimizes the balance between purification efficiency and process speed, with each stage tuned to remove specific contaminant size ranges.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This process efficiently extracts and purifies humic substances, producing a concentrated product for agricultural use and treated water that complies with environmental regulations, overcoming the limitations of previous methods.

Implementation Method 1

physical-chemical coagulation and flocculation

Methodology Applied
Scientific EffectCoagulation: Coagulation

Implementation Method 2

physical-chemical coagulation and flocculation

Methodology Applied
Scientific EffectFlocculation: Flocculation

Implementation Method 3

filtration through sand, microfiltration, and nanofiltration

Methodology Applied
Scientific EffectFiltration: Filter (physical)

Implementation Method 4

reverse osmosis

Methodology Applied
Scientific EffectReverse osmosis: Reverse Osmosis

Implementation Method 5

catalytic oxidation

Methodology Applied
Scientific EffectCatalytic oxidation: Catalysis

Implementation Method 6

ozone generator

Methodology Applied
Scientific EffectOzone generation: Ozone

Implementation Method 7

aeration tank

Methodology Applied
Scientific EffectAeration: Aeration

Implementation Method 8

continuous current source maintains the electric potential difference between 4 volts and 6 volts in the electrodes

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Implementation Method 9

ionic exchange resins

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Data Source

PatentEP3385230B1Process of extracting and purifying humic substances from sanitary landfill leachate
Publication Date: 2020.03.04 KUDRJAWZEW VLADIMIR
  • EP3385230B1 patent drawingFigure 1~4

AI summary

Patent of invention for process of extracting and purifying humic substances from sanitary landfill leachate comprising four steps: 1st physical-chemical step with the withdrawal of inert solids, 2nd step of filtration, 3rd step of purification of the humic substances with ionic exchange column followed by reverse osmosis and 4th step of catalytic oxidation and ammonolysis by cathodic reduction, obtaining treated effluents that complies with environmental legislation in terms of disposal or re-use of water.