Humidity Sensor Purging Sorbent Tubes

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Solution Overview

Problem

Current methods for purging sorbent tubes are inefficient in removing water, often requiring excessive purging time which can lead to loss of volatile gases and increased analytical time, and struggle to accurately determine the desired water level, affecting chromatography and sample analysis.

Innovation Solution

A device and system utilizing a humidity sensor fluidically coupled to a sorbent tube to detect the water level, with a processor controlling the purging gas flow to stop purging once a desired humidity level is reached, ensuring precise water removal and reducing unnecessary analytical time.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If purging is extended to ensure complete water removal, then water level reduction is improved, but volatile gas loss and analytical time increase

Engineering Contradiction:
Improvewater level controlVSAvoidanalytical time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The system employs a humidity sensor that provides real-time feedback on the water content within the sorbent tube during purging. This feedback mechanism allows the system to monitor water levels continuously and terminate the purging process precisely when the desired water level is achieved, preventing both over-purging (which would lose volatile gases) and under-purging (which would leave excess water). The humidity sensor data is fed back to the control system to dynamically adjust or stop the purging gas flow, optimizing both water removal efficiency and analytical time.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The invention replaces traditional mechanical or time-based purging control methods with an electronic sensing and control system. Instead of relying on fixed time intervals or mechanical indicators to determine when purging is complete, the system uses a humidity sensor to electronically detect water levels and a control system to automatically adjust the purging process. This substitution enables precise, real-time control that responds to actual water content rather than predetermined parameters.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Loss of substance

If purging time is reduced to preserve volatile gases, then volatile gas loss is minimized, but water removal efficiency decreases

Engineering Contradiction:
Improvevolatile gas lossVSAvoidwater level control
Core Design Contradiction:
Loss of substanceVSMeasurement precision

Solution Approach 1:

The humidity sensor provides continuous feedback on water content during the purging process, enabling the system to determine exactly when the desired water level is reached. This feedback allows for early termination of purging once the target is achieved, preventing unnecessary continued purging that would otherwise be required to ensure adequate water removal. The real-time monitoring ensures that purging stops at the optimal point rather than requiring excessive time to guarantee water removal.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The system replaces conservative, time-based purging protocols with an active sensing and control system. Instead of running purging for fixed extended periods to ensure water removal, the electronic humidity sensing system actively monitors water levels and dynamically controls the purging duration. This substitution enables the system to achieve adequate water removal with minimized purging time by responding to actual water content rather than predetermined time intervals.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Device complexity

If traditional purging methods are used without humidity monitoring, then device complexity is reduced, but water level determination accuracy deteriorates

Engineering Contradiction:
Improvesystem structureVSAvoidwater level detection
Core Design Contradiction:
Device complexityVSMeasurement precision

Solution Approach 1:

The invention replaces simple, unmonitored purging systems with an electronic sensing and control system. A humidity sensor is integrated into the sorbent tube assembly to electronically detect water levels in real-time. This electronic monitoring capability provides precise water level determination that cannot be achieved with traditional mechanical or unmonitored methods, enabling accurate control of the purging process based on actual water content rather than estimation or fixed protocols.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The humidity sensor acts as an intermediary element between the purging process and the control system. It provides real-time information about water content within the sorbent tube, serving as a mediator that translates physical water levels into measurable signals that the control system can use to adjust purging parameters. This intermediary sensing capability bridges the gap between the physical purging process and the decision-making control logic, enabling precise water level determination.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system effectively reduces water levels in sorbent tubes to a desired level, such as 3% relative humidity, minimizing the loss of volatile gases and optimizing analytical time by automatically halting purging when the target humidity is achieved.

Implementation Method 1

a humidity sensor configured to receive a fluid stream from the sorbent tube to determine the level of water in the sorbent tube

Methodology Applied
Scientific EffectHumidity detection: Hygrometer

Data Source

PatentUS10591936B2Devices, systems and methods for purging and loading sorbent tubes
Publication Date: 2020.03.17 PERKINELMER U S LLC
  • US10591936B2 patent drawing
  • US10591936B2 patent drawing
  • US10591936B2 patent drawing

AI summary

Certain embodiments described herein are directed to devices that can be used in purging and loading applications. In some examples, a device configured to purge a sorbent tube until a desired water level is reached is provided. In other examples, a device configured to load a sorbent tube with a desired water level is provided. Systems and methods using the devices are also described.