Water-in-oil explosive emulsion using hydrotreated vegetable oil

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Solution Overview

Problem

Emulsion-type explosives using renewable oils face instability due to differences in chemistry and behavior compared to traditional non-renewable oils, leading to emulsion breakdown and viscosity issues, necessitating the development of stable and environmentally friendly compositions.

Innovation Solution

Incorporating hydrotreated vegetable oil (HVO) as a fuel in combination with ammonium nitrate and secondary nitrate salts, such as calcium nitrate, to create stable explosive emulsions with adjustable viscosity, ensuring the emulsion remains stable and pumpable.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If renewable oils are used as fuel in emulsion explosives, then environmental sustainability is improved, but emulsion stability deteriorates

Engineering Contradiction:
Improveenvironmental impactVSAvoidemulsion stability
Core Design Contradiction:
Object-affected harmful factorsVSStability of the object's composition

Solution Approach 1:

The patent modifies the chemical composition parameters by introducing secondary nitrate salts (calcium nitrate, sodium nitrate, or potassium nitrate) at concentrations of 5-50 wt% in the oxidizer phase. This parameter change resolves the instability caused by renewable oils while maintaining the environmental benefits, as the secondary salts adjust the chemical environment to be compatible with renewable fuel chemistry

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite oxidizer phase combining primary (ammonium nitrate) and secondary nitrate salts, and a composite fuel phase combining renewable oils with traditional emulsifiers. This composite approach allows the system to benefit from both renewable sustainability and traditional stability mechanisms, resolving the contradiction between environmental impact and emulsion stability

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If renewable oils are used as fuel in emulsion explosives, then sustainability is improved, but viscosity control deteriorates

Engineering Contradiction:
Improveenvironmental impactVSAvoidviscosity control
Core Design Contradiction:
Object-affected harmful factorsVSEase of operation

Solution Approach 1:

The patent uses secondary nitrate salts as viscosity modifiers that change the physical parameters of the emulsion. By adjusting the concentration of secondary salts (5-50 wt%), the viscosity can be controlled to achieve pumpable consistency while maintaining renewable fuel composition, thus resolving the viscosity control issue without sacrificing sustainability

Inventive Principle:
Principle #35Parameter changes

3Stability of the object's composition

If chemically processed renewable oils are used, then emulsion stability is improved, but emulsification process deteriorates

Engineering Contradiction:
Improveemulsion stabilityVSAvoidemulsification process
Core Design Contradiction:
Stability of the object's compositionVSEase of manufacture

Solution Approach 1:

The patent introduces secondary nitrate salts as intermediary substances that mediate between the renewable fuel phase and oxidizer phase. These salts act as chemical intermediaries that facilitate emulsification by creating a compatible interface, thus improving stability while maintaining ease of manufacture through simplified mixing processes

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of HVO and secondary nitrate salts in the emulsion composition results in stable, green explosive emulsions with customizable viscosity, overcoming the instability issues associated with renewable oils and providing a more sustainable alternative.

Implementation Method 1

the inventors have surprisingly found that the viscosity of the explosive emulsion could be reduced by including a HVO as defined herein in the fuel composition

Methodology Applied
Scientific EffectViscosity reduction:

Implementation Method 2

stable explosive emulsions comprising chemically processed renewable oils as fuel can be obtained by adding a suitable amount of one or more secondary salts, in particular calcium nitrate

Methodology Applied
Scientific EffectEmulsion stabilization: Emulsion

Data Source

PatentUS20240076247A1Emulsion-type explosives of the water-in-oil type
Publication Date: 2024.03.07 YARA INTERNATIONAL ASA

AI summary

An explosive emulsion composition of the water-in-oil type, comprising:between 80 wt. % and 95 wt. % of an oxidizer phase in view of the total weight of the emulsion composition, comprisingat least 40 wt. % of ammonium nitrate (AN), andat least 5 wt. % of a secondary nitrate salt,in view of the total weight of the oxidizer phase composition, and between 5 wt. % and 20 wt. % of an organic phase in view of the total weight of the emulsion composition, the organic phase comprising:between 12 wt. % and 50 wt. % of one or more emulsifiers,between 50 wt. % and 88 wt. % of a fuel composition,in view of the total weight of the organic phase composition,characterized in that the fuel composition comprises between 20 wt. % and 100 wt. % of a hydrotreated vegetable oil (HVO), in view of the total weight of the fuel composition.