Hydrogen Embrittlement Detection via Static Load Bending

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Solution Overview

Problem

Current methods for determining hydrogen embrittlement in metals are time-consuming, often taking up to 200 hours, making it difficult to assess contamination levels in real-time, and are not efficient in detecting the presence of hydrogen-induced brittleness in plated samples.

Innovation Solution

A method and system that involves a calibration phase to determine the average distance at which unplated samples fracture, followed by a testing phase where plated samples are subjected to a static load at a predetermined percentage of this distance to assess hydrogen embrittlement, allowing for real-time determination within 8 hours.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If known stress test methods are used to determine hydrogen embrittlement, then measurement precision is improved, but loss of time increases significantly (up to 200 hours)

Engineering Contradiction:
Improvehydrogen embrittlement detection accuracyVSAvoidtesting duration
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent applies preliminary action by pre-calibrating the test system with unplated samples to establish a baseline fracture distance. This calibration phase is performed once, and the resulting reference value is stored for use in subsequent plated sample tests, eliminating the need to repeat the full calibration process for each test and significantly reducing overall testing time

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent segments the testing process into distinct phases: a calibration phase using unplated samples to determine baseline fracture characteristics, and a testing phase using plated samples with predetermined load percentages. This segmentation allows the time-consuming calibration to be performed once rather than repeatedly for each sample type, reducing total testing duration while maintaining measurement precision

Inventive Principle:
Principle #1Segmentation

2Productivity

If prolonged use of plating solution is allowed, then productivity is improved, but object-generated harmful factors increase (contaminant concentration increases)

Engineering Contradiction:
Improveplating solution utilization efficiencyVSAvoidcontaminant concentration in plating solution
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent implements feedback by using the fracture distance measurements from plated samples to monitor the condition of the plating solution over time. As contaminants accumulate in the plating solution, the hydrogen embrittlement resistance changes, which is detected through the fracture distance measurements. This feedback mechanism allows operators to determine when the plating solution needs replacement or regeneration, optimizing both productivity and solution quality

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The plating solution effectively monitors its own condition through the test samples. The samples undergo the same plating process and are then tested for hydrogen embrittlement, allowing the system to self-assess the solution's contamination level without requiring separate analytical instrumentation or additional testing equipment

Inventive Principle:
Principle #25Self-service

3Object-generated harmful factors

If plating layer porosity is decreased to prevent contamination, then object-generated harmful factors are reduced, but object-affected harmful factors increase (hydrogen removal efficiency decreases)

Engineering Contradiction:
Improvecontaminant release into plating solutionVSAvoidhydrogen embrittlement resistance
Core Design Contradiction:
Object-generated harmful factorsVSObject-affected harmful factors

Solution Approach 1:

The patent applies parameter changes by measuring fracture distance rather than relying on fixed load thresholds. This parameter change allows the test to adapt to varying plating conditions, including different porosity levels. The predetermined percentage of baseline ultimate failure distance accounts for variations in plating layer properties, enabling accurate hydrogen embrittlement assessment regardless of the porosity-contamination trade-off present in the plating process

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables rapid detection of hydrogen embrittlement in plated samples, facilitating the assessment of plating solution contamination and improving production efficiency by providing a quick indication of hydrogen-induced brittleness.

Implementation Method 1

moving the second holding member towards the first holding member to bend the plated sample; and applying a static load to the plated sample

Methodology Applied
Scientific EffectMechanical Force: Mechanical Force

Implementation Method 2

Hydrogen embrittlement refers to a process that causes a metal or metal alloy, such as steel, to become brittle and susceptible to fracture when exposed to a quantity of hydrogen and subjected to a tensile load

Methodology Applied
Scientific EffectFracture Mechanics: Fracture Mechanics

Data Source

PatentEP2772756B1Method and systems for determining hydrogen embrittlement
Publication Date: 2021.09.15 THE BOEING CO
  • EP2772756B1 patent drawingFigure 1
  • EP2772756B1 patent drawingFigure 2
  • EP2772756B1 patent drawingFigure 3

AI summary

A method for use in determining hydrogen embrittlement in a plated sample is provided. The method includes positioning the plated sample between a first holding member and a second holding member, moving the second holding member towards the first holding member to bend the plated sample, and applying a static load to the plated sample for a predetermined duration of time. The static load is applied by bending the plated sample to a distance between the first and second holding members that is a predetermined percentage of a baseline ultimate failure distance of the plated sample.