Hydrogen Tank Multilayer Liner for Heat and Permeation Resistance

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Solution Overview

Problem

Existing hydrogen tanks face challenges with low thermal resistance, high permeability to hydrogen, and limited mechanical strength, especially at extreme temperatures, which hinder efficient hydrogen storage and filling speed.

Innovation Solution

A multilayer structure comprising a sealing layer made of polyamide, catalyst, thermal stabilizer, oligo- or poly-carbodiimide, and optionally polyolefin, combined with a composite reinforcing layer of fibrous material impregnated with epoxy resin, enhances mechanical strength and thermal resistance, reducing hydrogen permeability and allowing higher filling speeds.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If HDPE is used as the liner material, then the manufacturing process is simple, but the thermal resistance is insufficient and hydrogen permeability is high

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidthermal resistance
Core Design Contradiction:
Ease of manufactureVSTemperature

Solution Approach 1:

The patent uses a composite liner structure combining PA11 polymer matrix with impact modifier and plasticizer additives to achieve both manufacturability and thermal resistance. This composite approach allows the material to maintain processability while achieving the required thermal performance for hydrogen storage tanks.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent modifies the chemical composition parameters of the liner material by incorporating specific ratios of impact modifier (15-50%) and plasticizer (1-3%), which changes the material properties to achieve both thermal resistance and manufacturability. This parameter optimization resolves the contradiction between ease of manufacture and thermal resistance.

Inventive Principle:
Principle #35Parameter changes

2Temperature

If PA6 is used as the liner material, then the thermal resistance improves, but the resistance to cold deteriorates

Engineering Contradiction:
Improvethermal resistanceVSAvoidresistance to cold
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The patent changes the base polymer from PA6 to PA11, which fundamentally alters the temperature-performance characteristics. PA11 provides both thermal resistance and cold resistance, eliminating the trade-off present in PA6. The addition of impact modifier further enhances cold resistance while maintaining thermal properties.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent adds impact modifier specifically to improve cold-temperature performance in the liner material. This localized property enhancement addresses the cold resistance issue without compromising the thermal resistance achieved by the PA11 base material.

Inventive Principle:
Principle #3Local quality

3Productivity

If the filling speed is increased, then the productivity improves, but the temperature increases causing thermal degradation

Engineering Contradiction:
Improvefilling speedVSAvoidthermal resistance
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The patent adds plasticizer to the liner composition, which modifies the thermal properties and thermal stability of the material. This allows the liner to withstand higher temperatures generated during fast filling operations, enabling increased productivity without thermal degradation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses a thermoplastic liner that can be manufactured with controlled thickness and properties optimized for fast filling. The liner acts as a sacrificial thermal management component that protects the hydrogen storage system during high-speed filling, allowing productivity improvement.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

4Strength

If the viscosity is increased to improve mechanical strength, then the strength improves, but the ease of manufacture deteriorates

Engineering Contradiction:
Improvemechanical strengthVSAvoidtransformability
Core Design Contradiction:
StrengthVSEase of manufacture

Solution Approach 1:

The patent adds plasticizer to the polymer composition, which reduces the viscosity of the molten material during processing. This allows the material to be easily formed and molded despite having high molecular weight and inherent strength, resolving the contradiction between strength and ease of manufacture.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The structure achieves improved mechanical strength, reduced hydrogen permeability, and increased operating temperature up to 120°C, enabling faster hydrogen filling without significant manufacturing temperature increases.

Implementation Method 1

at least one oligo- or poly-carbodiimide... which has hydrogen barrier properties, good flexibility, and durability at low temperature

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 2

a composition consisting of PA11, from 15 to 50% of an impact modifier and from 1 to 3% of plasticizer, or devoid of plasticizer... at least one catalyst

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

at least one thermal stabilizer... Thermal resistance at 120° C.

Methodology Applied
Scientific EffectThermal stabilization:

Data Source

PatentUS12485657B2Multi-layer structure for storing hydrogen
Publication Date: 2025.12.02 ARKEMA FRANCE SA

AI summary

Multi-layer structure intended for storing hydrogen, including, from the inside out, a sealing layer and a composite reinforcing layer, the innermost composite reinforcing layer being wound around the outermost adjacent sealing layer, at least the innermost sealing layer being made of a composition including: a. 20.5 to 99.845% by weight of a polyamide; b. 0.005 to 0.5% by weight of a catalyst; c. 0.05 to 1% by weight of a heat stabilizer; d. 0.1 to 3% by weight of a oligo- or poly-carbodiimide; e. 0 to 1.5% by weight of a plasticiser; f. 0 to less than 15% by weight of a polyolefin; g. 0 to 30% of an additive, and at least one of the composite reinforcing layers of a fibrous material in the form of continuous fibres impregnated with a composition including at least one polymer P2j, j=1 to m, m being the number of reinforcing layers.