Hydrohalofluoroolefin Isomerization Catalyst Moisture Control

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Solution Overview

Problem

Existing methods for isomerizing hydrohalofluoroolefins face challenges in maintaining catalyst performance due to moisture levels, leading to inefficiencies in converting E/Z isomers.

Innovation Solution

The method involves adjusting the moisture concentration of hydrohalofluoroolefin isomers to 100 ppm or lower before contacting them with a catalyst in a gas phase, using metal oxide or fluorinated metal compounds, and optimizing temperature and contact time to suppress catalyst deactivation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If hydrohalofluoroolefin isomerization is conducted using conventional catalysts without moisture control, then the isomerization reaction can proceed, but catalyst performance deteriorates due to moisture-induced deactivation

Engineering Contradiction:
Improvecatalyst performanceVSAvoidmoisture deactivation
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent applies preliminary action by controlling moisture content in the hydrohalofluoroolefin feedstock to 100 ppm or lower before the isomerization reaction begins. This preventive measure ensures catalyst performance is maintained from the start of the reaction, avoiding moisture-induced deactivation that would otherwise occur during conventional isomerization processes

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent changes the moisture concentration parameter of the feedstock to a specific range (100 ppm or lower). This parameter modification fundamentally alters the reaction conditions to prevent catalyst deactivation, transforming a harmful moisture environment into a controlled, catalyst-friendly environment that maintains reliable catalytic activity throughout the isomerization process

Inventive Principle:
Principle #35Parameter changes

2Reliability

If moisture concentration is reduced to maintain catalyst performance, then catalyst deactivation is suppressed, but additional moisture control steps are required in the process

Engineering Contradiction:
Improvecatalyst performanceVSAvoidmoisture control process
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent modifies the moisture concentration parameter of the feedstock to 100 ppm or lower, creating optimized reaction conditions that maintain catalyst performance. This parameter change enables the use of simpler catalyst systems and reduces the need for complex moisture removal equipment downstream, as the controlled moisture level prevents catalyst deactivation in the first place

Inventive Principle:
Principle #35Parameter changes

3Productivity

If conventional isomerization methods are used without moisture control, then the process is simpler to operate, but isomerization efficiency decreases due to catalyst deactivation

Engineering Contradiction:
Improveisomerization efficiencyVSAvoidmoisture control requirement
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The patent implements preliminary moisture control to maintain feedstock moisture at 100 ppm or lower before isomerization begins. This preliminary action prevents catalyst deactivation, ensuring high isomerization efficiency throughout the reaction process while avoiding the need for complex operational adjustments during reactor operation

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

By changing the moisture concentration parameter to 100 ppm or lower, the patent creates optimized reaction conditions that maintain high catalyst activity and isomerization efficiency. This parameter modification transforms the process into one that is both efficient and operationally straightforward, as the controlled moisture level prevents catalyst deactivation without requiring complex real-time adjustments

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively maintains catalyst performance, enhancing the efficiency of isomerization by reducing moisture-related deactivation and improving the yield of target hydrohalofluoroolefin isomers.

Implementation Method 1

contacting a composition that contains at least a hydrohalofluoroolefin isomer (isomer 1) and that has been adjusted to 100 ppm or lower in moisture concentration, with a catalyst in a gas phase, thereby obtaining a product

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP3296282B1Method for producing hydrohalofluoroolefins
Publication Date: 2020.07.29 CENT GLASS CO LTD
  • EP3296282B1 patent drawingFigure 1~2
  • EP3296282B1 patent drawingFigure 3~4
  • EP3296282B1 patent drawingFigure 5

AI summary

[TASK] It is a task to provide a method for efficiently isomerizing a hydrohalofluoroolefin isomer (isomer 1) by suppressing lowering of catalyst performance to produce the corresponding hydrohalofluoroolefin isomer (isomer 2). [SOLVING MEANS] A method for isomerizing a hydrohalofluoroolefin isomer (isomer 1) to produce a corresponding hydrohalofluoroolefin isomer (isomer 2), comprising step 1 of contacting a composition that contains at least a hydrohalofluoroolefin isomer (isomer 1) and that has been adjusted to 100 ppm or lower in moisture concentration, with a catalyst in a gas phase, thereby obtaining a product.