Hydrosilylation-Curable Silicone Composition for Low-Temperature Curing

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Solution Overview

Problem

Hydrosilylation-curable silicone compositions face challenges in maintaining storage stability and preventing surface wrinkling when cured at low temperatures, while achieving good curability.

Innovation Solution

Incorporating a maleate compound and a hydrosilylation inhibitor in specific ppm ranges, along with an organopolysiloxane, organohydrogenpolysiloxane, and a hydrosilylation catalyst, to form a composition that can be cured at low temperatures without surface wrinkling.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the curing temperature is reduced and curing time is shortened, then curability is improved, but storage stability deteriorates markedly

Engineering Contradiction:
ImprovecurabilityVSAvoidstorage stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent applies parameter changes by carefully controlling the concentrations of two different inhibitors (maleate compound at 50-6000 ppm and hydrosilylation inhibitor at 200-20000 ppm) to achieve the optimal balance between storage stability and curability. This dual-inhibitor system with specific concentration ranges allows the composition to maintain stability during storage while enabling rapid curing when activated.

Inventive Principle:
Principle #35Parameter changes

2Use of energy by stationary object

If the curing temperature is reduced, then energy consumption is decreased, but surface wrinkling of cured products is promoted

Engineering Contradiction:
Improvecuring energyVSAvoidsurface quality
Core Design Contradiction:
Use of energy by stationary objectVSManufacturing precision

Solution Approach 1:

The patent uses parameter changes by optimizing the concentration ratio between the maleate compound and hydrosilylation inhibitor, along with controlling the organohydrogenpolysiloxane content, to enable low-temperature curing without surface wrinkling. The specific parameter ranges provided ensure that the curing reaction proceeds uniformly even at reduced temperatures.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs a composite inhibitor system combining two different types of inhibitors (maleate compound and hydrosilylation inhibitor) with distinct mechanisms of action. This composite approach provides synergistic effects that prevent surface wrinkling while enabling low-temperature curing, achieving better performance than single-inhibitor systems.

Inventive Principle:
Principle #40Composite materials

3Device complexity

If a single hydrosilylation inhibitor is used, then the composition is simple, but it is difficult to consistently achieve both good curability and prevent surface wrinkling

Engineering Contradiction:
Improvecomposition complexityVSAvoidsurface quality consistency
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The patent implements a composite inhibitor system using two different inhibitors (maleate compound and hydrosilylation inhibitor) that work through different mechanisms. This composite approach provides consistent control over both curability and surface quality, overcoming the limitations of single-inhibitor systems while maintaining manageable composition complexity through defined concentration ranges.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition exhibits good storage stability and prevents surface wrinkling during low-temperature curing, maintaining excellent curability and mechanical characteristics of the cured product.

Implementation Method 1

at least one hydrosilylation inhibitor is added to adjust curability and storage stability of the compositions

Methodology Applied
Scientific EffectHydrosilylation inhibition:

Implementation Method 2

a hydrosilylation catalyst, in an amount sufficient to accelerate curing of the composition

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

Hydrosilylation-curable silicone compositions form cured products having excellent characteristics

Methodology Applied
Scientific EffectHydrosilylation reaction: Chemical Bonding

Data Source

PatentUS11377557B2Hydrosilylation-curable silicone composition
Publication Date: 2022.07.05 DDP SPECIALTY ELECTRONIC MATERIALS US 9 LLC

AI summary

The present invention relates to a hydrosilylation-curable silicone composition comprising: a maleate compound, and a hydrosilylation inhibitor other than the maleate compound, wherein the content of the maleate compound is in an amount of 50 to 6,000 ppm and the content of the hydrosilylation inhibitor is in an amount of 200 to 20,000 ppm, with respect to the present composition in terms of mass units, respectively. The hydrosilylation-curable silicone composition exhibits good storage stability, and can be cured to form a cured product that suffers no surface wrinkling.