ICP Reactor Gas Pipe Segmentation for Silicon Nanoparticle Grain Control

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Solution Overview

Problem

Conventional ICP-based apparatuses for producing silicon nanoparticles face challenges in controlling grain size due to wide plasma diffusion, leading to aggregation and reduced production yield.

Innovation Solution

The apparatus features a plasma reactor with first and second gas supply pipes arranged in an alternative pattern, extending the first gas pipes to the plasma initiation region and keeping the second gas pipes distal, which enhances uniform plasma reaction and plasma density, minimizing expansion and aggregation through cooling.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If a conventional ICP-based apparatus with a reactor wound with an ICP coil around the outer circumference is used, then silicon nanoparticles can be produced, but the plasma reaction area becomes wide due to plasma diffusion, making it difficult to control the grain size of silicon nanoparticles

Engineering Contradiction:
Improvegrain size controlVSAvoidplasma reaction area
Core Design Contradiction:
Manufacturing precisionVSArea of stationary object

Solution Approach 1:

The gas supply system is segmented into multiple first gas pipes and second gas pipes arranged in an alternative pattern. The first gas pipes extend to the plasma initiation region while the second gas pipes remain distal, creating distinct reaction zones that confine plasma diffusion and improve grain size control.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different regions of the reactor are provided with different gas supply characteristics. The plasma initiation region receives first gas through extended pipes for nanoparticle formation, while other regions receive second gas through distal pipes for surface reaction, creating localized reaction conditions that control plasma density and grain size.

Inventive Principle:
Principle #3Local quality

2Productivity

If plasma diffusion occurs inside the reactor causing a wide reaction area, then silicon nanoparticles can be produced, but the reaction time extends, making it difficult to control the grain size and lowering the production yield

Engineering Contradiction:
Improveproduction yieldVSAvoidreaction time
Core Design Contradiction:
ProductivityVSDuration of action of moving object

Solution Approach 1:

The reactor is segmented into a plasma initiation region and other regions, with gas supply pipes strategically positioned to create confined reaction zones. This segmentation reduces plasma diffusion distance, shortens reaction time, and improves production yield by preventing excessive plasma expansion.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The first gas pipes are extended to the plasma initiation region before plasma formation occurs, pre-positioning the gas supply to ensure rapid and localized plasma generation. This preliminary positioning reduces the time required for plasma establishment and nanoparticle formation, improving overall reaction efficiency.

Inventive Principle:
Principle #10Preliminary action

3Manufacturing precision

If the second gas is supplied for the surface reaction of silicon nanoparticles, then surface modification can be achieved, but the wide reaction area caused by plasma diffusion extends the reaction time and lowers production yield

Engineering Contradiction:
Improvesurface reaction controlVSAvoidproduction yield
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The second gas pipes are positioned distal from the plasma reaction part, supplying second gas to specific regions for surface reaction. This localized gas supply enables precise control of surface modification while confining the reaction area, preventing plasma diffusion from extending the overall reaction time and maintaining high production yield.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration allows precise control over grain size distribution and increases production yield by preventing secondary aggregation and optimizing plasma retention time.

Implementation Method 1

a plasma reaction part with an ICP coil wound around the outer wall thereof

Methodology Applied
Scientific EffectInductive coupled plasma: Electromagnetic Induction

Implementation Method 2

a cooling part for cooling produced silicon nanoparticles, and a collection part for collecting particles captured by mesh filters

Methodology Applied
Scientific EffectCooling: Cooling

Data Source

PatentUS9802826B2Apparatus for producing silicon nanoparticle using inductive coupled plasma
Publication Date: 2017.10.31 KOREA INST OF ENERGY RES
  • US9802826B2 patent drawing
  • US9802826B2 patent drawing
  • US9802826B2 patent drawing

AI summary

An apparatus for producing silicon nanoparticles using ICP includes a gas supply part in which first and second pipes for introducing a respective first and second gas into the plasma reactor therethrough are arranged alternately, the first pipes extending from an inlet of the reactor to a plasma initiation region; a plasma reaction part having an ICP coil wound therearound in which the particles are formed as the gases introduced through the respective pipes undergo a plasma reaction; and a collection part for collecting the particles. The apparatus can fully mix the gases introduced through the first gas supply pipes, thus allowing for uniform plasma reaction between the first and second gas, minimizing plasma expansion to increase plasma density within short retention time, easily controlling the size distribution by quenching and capturing nanoparticles, and improving the production yield by preventing the secondary aggregation of particles with cooling gas.