IGBT Silicon Wafer COP Reduction via Annealing

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Solution Overview

Problem

Silicon wafers produced by the Czochralski method (CZ method) for insulated gate bipolar transistors (IGBTs) face issues with gate oxide integrity, resistivity fluctuations, recombination lifetime deterioration, and the presence of crystal-originated particles (COPs), which hinder their suitability as substrates due to high oxygen concentrations and impurity segregation.

Innovation Solution

A method involving the growth of silicon ingots with low interstitial oxygen concentrations, neutron irradiation for homogeneous phosphorus doping, and annealing in an oxidizing atmosphere to form a silicon oxide layer that fills COPs, along with nitrogen doping to reduce COP sizes and inhibit slip dislocations, and forming a strained layer as a gettering layer to remove heavy metals.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If silicon wafers are produced by the CZ method to achieve large diameter and mass production, then productivity and ease of manufacture are improved, but crystal-originated particles (COPs) are generated that deteriorate gate oxide integrity

Engineering Contradiction:
Improvemass production capabilityVSAvoidgate oxide integrity
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent applies preliminary action by performing heat treatment on the silicon wafer before oxide film formation to eliminate COPs. The heat treatment process is conducted in advance to prevent COPs from being captured in the oxide film layer during subsequent thermal oxidation, thereby maintaining gate oxide integrity while preserving the productivity benefits of CZ method mass production

Inventive Principle:
Principle #10Preliminary action

2Reliability

If oxygen concentration in CZ silicon is controlled to eliminate COPs, then gate oxide integrity is improved, but recombination lifetime deteriorates due to oxide precipitation

Engineering Contradiction:
Improvegate oxide integrityVSAvoidrecombination lifetime
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The patent applies parameter changes by precisely controlling the oxygen concentration parameter to a specific range (1×10^18 to 5×10^18 atoms/cm³) and adjusting the heat treatment temperature parameter (900°C to 1200°C) to achieve the optimal balance. This parameter optimization eliminates COPs while preventing excessive oxide precipitation that would deteriorate recombination lifetime, thus resolving the contradiction between gate oxide integrity and carrier lifetime

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If phosphorus doping is used to control resistivity in CZ silicon, then electrical properties are improved, but resistivity becomes non-uniform due to segregation

Engineering Contradiction:
Improveresistivity controlVSAvoidresistivity uniformity
Core Design Contradiction:
Manufacturing precisionVSStability of the object's composition

Solution Approach 1:

The patent applies feedback by implementing a two-stage doping strategy where phosphorus is added during crystal growth and additional phosphorus is introduced through heat treatment. The process monitors and adjusts doping levels to compensate for segregation effects, ensuring uniform resistivity distribution while maintaining precise electrical property control

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in silicon wafers with reduced COPs, stable resistivity, and improved recombination lifetime, making them suitable for IGBT applications by enhancing gate oxide integrity and reducing thermal donor generation.

Implementation Method 1

annealing of the wafer in an oxidizing atmosphere, thereby forming a silicon oxide layer on a surface of the silicon wafer

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 2

it is possible to transform a predetermined amount of the silicon atoms into phosphorus atoms by irradiating neutrons to the silicon ingot

Methodology Applied
Scientific EffectNeutron transmutation doping: Nuclear Fission

Implementation Method 3

forming a strained layer as a gettering layer to remove heavy metals

Methodology Applied
Scientific EffectGettering: Gettering

Data Source

PatentEP1732114B1Method for producing silicon wafer for IGBT
Publication Date: 2018.12.05 SUMCO CORP
  • EP1732114B1 patent drawingFigure 1
  • EP1732114B1 patent drawingFigure 2A~2B
  • EP1732114B1 patent drawingFigure 3A~3D

AI summary

A silicon wafer for an IGBT is produced by forming an ingot having an interstitial oxygen concentration [Oi] of not more than 7.0 × 1017atoms/cm3 by the Czochralski method; doping phosphorus in the ingot by neutron beam irradiation to the ingot; slicing a wafer from the ingot; performing annealing of the wafer in an oxidizing atmosphere containing at least oxygen at a temperature satisfying a predetermined formula; and forming a polysilicon layer or a strained layer on one side of the wafer.