III/V Semiconductor Epitaxy on Silicon Buffer Layers

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Solution Overview

Problem

The integration of III/V semiconductor layers on silicon substrates is hindered by dislocation and anti-phase defects due to lattice constant differences and thermal expansion coefficient mismatches, making it challenging to produce high-performance, long-lasting components on large 300 mm Si substrates while maintaining economic viability.

Innovation Solution

A method involving epitaxial deposition of III/V semiconductor layers on Si wafers with a specialized surface preparation, including deoxidation, silicon buffer layer growth, and etching, followed by low-temperature III/V film growth and subsequent high-temperature crystallization, to minimize dislocation and anti-phase defects, using a CCS Crius epitaxy system for precise temperature control on 300 mm substrates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If III/V semiconductor layers are deposited on silicon substrates, then new functionalities and improved performance are achieved, but dislocation and anti-phase defects form due to lattice constant differences

Engineering Contradiction:
Improveintegration of new materialsVSAvoiddefect formation
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

A silicon buffer layer is introduced as an intermediary between the silicon substrate and the III/V semiconductor layer. This buffer layer acts as a mediator that accommodates the lattice constant mismatch, preventing dislocation defects from propagating into the active III/V device layers while enabling successful integration of new materials.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The silicon buffer layer is grown in advance before depositing the III/V semiconductor layers. This preliminary action prepares the substrate surface with appropriate crystal structure and reduces thermal stress, preventing anti-phase defects and dislocations before the actual device layers are formed.

Inventive Principle:
Principle #10Preliminary action

2Ease of manufacture

If monolithic growth of III/V layers on Si substrates is used, then production costs are reduced, but dislocation defects still form making high-performance components difficult to implement

Engineering Contradiction:
Improveproduction costVSAvoidcomponent quality
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The silicon buffer layer serves as a cost-effective intermediary that enables monolithic growth while maintaining high component quality. It prevents dislocation defects at a relatively low additional cost compared to alternative approaches, achieving both economic viability and high manufacturing precision.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Adaptability or versatility

If standard CMOS substrates are used, then compatibility with current technology is maintained, but anti-phase defects form quickly during III/V layer deposition

Engineering Contradiction:
Improvecompatibility with CMOSVSAvoiddefect formation rate
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The silicon buffer layer acts as a protective intermediary between the standard CMOS substrate and the III/V layers. It maintains compatibility with existing CMOS manufacturing processes while simultaneously preventing anti-phase defects during the deposition of new material layers.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The buffer layer is grown in advance to establish a stable crystal structure that is compatible with standard CMOS substrates. This preliminary preparation prevents rapid defect formation during subsequent III/V layer deposition, enabling reliable integration.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables the deposition of dislocation-free III/V semiconductor materials on misoriented silicon substrates up to 300 mm in diameter, ensuring compatibility with current CMOS technology and reducing production costs, thus facilitating the integration of III/V components like transistors, laser diodes, LEDs, and solar cells.

Implementation Method 1

a Si layer is deposited on the surface of the deoxidized Si wafer... a silicon buffer layer is grown

Methodology Applied
Scientific EffectEpitaxy: Epitaxy

Implementation Method 2

using a CCS Crius epitaxy system... epitaxial deposition of III/V semiconductor layers

Methodology Applied
Scientific EffectVapor phase deposition: Physical Vapour Deposition

Implementation Method 3

the surface of the Si layer undergoes an etching process stage using an active Cl-containing gas

Methodology Applied
Scientific EffectChemical etching:

Implementation Method 4

a layer of a III/V semiconductor is grown epitaxially... a layer of a III/V semiconductor, identical to or different from the III applied in step D)/V semiconductor, grown epitaxially

Methodology Applied
Scientific EffectEpitaxy: Epitaxy

Implementation Method 5

epitaxial deposition of III/V semiconductor layers... using a CCS Crius epitaxy system

Methodology Applied
Scientific EffectVapor phase deposition: Physical Vapour Deposition

Implementation Method 6

low-temperature III/V film growth and subsequent high-temperature crystallization

Methodology Applied
Scientific EffectThermal diffusion: Diffusion

Implementation Method 7

subsequent high-temperature crystallization

Methodology Applied
Scientific EffectCrystallization: Crystallisation

Data Source

PatentEP2695180B1Method for producing a iii/v si template
Publication Date: 2016.03.30 NASP IIIV

AI summary

The invention relates to a method for producing a monolithic template containing an Si wafer having a layer of a III/V semiconductor that is epitaxially applied to a surface of the Si wafer, wherein the III/V semiconductor comprises a lattice constant that deviates from the constant of the Si by less than 10%, comprising the following steps: A) the surface of the Si wafer is optionally deoxidized, B) an Si layer is optionally grown epitaxially on the surface of the deoxidized Si wafer, C) the surface of the Si wafer or the surface of the Si layer is optionally subjected to an etching and/or bake-out step, D) a layer made of a III/V semiconductor is epitaxially grown on the surface of the Si wafer or a surface produced in steps A) to C) at a wafer temperature of 350-650 °C, a growth rate of 0.1-2 μm/h, and a layer thickness of 1-100 nm, E) a layer made of a III/V semiconductor equal to or different from the III/V semiconductor applied in step D) is epitaxially grown on the layer obtained in step D) at a wafer temperature of 500-800 °C, a growth rate of 0.1-10 μm/h, and a layer thickness of 10-150 nm.