Imaging Mass Spectrometer Multi-Spot Laser Analysis

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Solution Overview

Problem

Current mass spectrometry methods for analyzing biological samples are time-consuming, requiring multiple measurements at spaced-apart spots, which is inefficient and competitive for expensive equipment.

Innovation Solution

An imaging mass spectrometer that simultaneously provides energy to multiple spots on a sample using a laser at an angle perpendicular to the surface, with grid electrodes to focus ions and a Time Of Flight (TOF) analyzer to detect arrival time and spot origin of ions, enabling parallel analysis of multiple spots.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If multiple measurements are made at spaced apart spots to determine the composition of the whole sample, then measurement precision is improved, but loss of time increases

Engineering Contradiction:
Improvecomposition analysis accuracyVSAvoidanalysis time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The sample plate is divided into multiple discrete spots that can be independently irradiated. The laser system is segmented into multiple beams that simultaneously target different spots, allowing parallel analysis of multiple sample regions without compromising measurement precision while significantly reducing total analysis time

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Multiple laser beams are combined to simultaneously irradiate multiple spots on the sample plate. The ion detection system merges signals from all spots, enabling comprehensive composition analysis of the entire sample in a single measurement cycle, thereby eliminating the time-consuming sequential measurement process

Inventive Principle:
Principle #5Merging (Combining)

2Measurement precision

If a laser is used to ionize the sample by Matrix Assisted Laser Desorption, then measurement precision is improved, but device complexity increases

Engineering Contradiction:
Improveion detection accuracyVSAvoidlaser system complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

A microlens array is introduced as an intermediary optical element that receives laser energy from a single source and automatically distributes it into multiple focused beams. This intermediary component simplifies the overall laser system architecture by eliminating the need for multiple independent laser sources while maintaining the precision required for MALDI ionization at each spot

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The complex mechanical system of multiple independent laser sources is replaced with a single laser source combined with an optical microlens array system. This substitution maintains the functional capability of simultaneous multi-spot irradiation while significantly reducing device complexity and cost

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces analysis time by allowing simultaneous analysis of multiple spots, increasing sample throughput and improving efficiency in mass spectrometry.

Implementation Method 1

energy source adapted to substantially simultaneously provide energy to multiple spots on a sample to produce ions from the sample by a desorption process; Desorption of the ions can occur by Matrix Assisted Laser Desorption lonisation

Methodology Applied
Scientific EffectMatrix Assisted Laser Desorption: Laser Ablation

Implementation Method 2

one or more grid electrodes to focus the ions resulting from the desorption process

Methodology Applied
Scientific EffectIon focusing: Electrostatic Lens

Implementation Method 3

an analyser adapted to detect the arrival time and spot origin of ions resulting from said desorption process; The analyser can comprise a TOF

Methodology Applied
Scientific EffectTime of Flight: Time of Flight

Data Source

PatentEP2795659B1An imaging mass spectrometer and a method of mass spectrometry
Publication Date: 2019.12.11 MICROMASS UK LTD
  • EP2795659B1 patent drawingFigure 1~2
  • EP2795659B1 patent drawingFigure 3~4
  • EP2795659B1 patent drawingFigure 5~6

AI summary

An imaging mass spectrometer comprising an energy source adapted to substantially simultaneously provide energy to multiple spots on a sample to produce ions from the sample by a desorption process; and an analyzer adapted to detect the arrival time and spot origin of ions resulting from said desorption process.