Inert Gas Atmosphere Control for 3D Metal Printing

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Solution Overview

Problem

Current 3D laser printing methods using metallic powders face issues with contamination from oxygen, water, and hydrocarbons, leading to reduced yields, poor product quality, and the need for extensive post-processing due to inadequate atmosphere control and impurity management.

Innovation Solution

Implementing a system with a 3D printer and gas supply system that uses inert gases with a purity of 99.995% or higher, combined with gas sensors to dynamically adjust the gas flowrate and incorporate gas purifiers to maintain a clean atmosphere during printing and weld overlay operations.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If inert gas with high purity (99.995% or higher) is used, then product quality and mechanical properties are improved, but system complexity and cost increase

Engineering Contradiction:
Improveproduct qualityVSAvoidsystem complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The system performs preliminary purging of the printing chamber and powder feed system with high-purity inert gas before the additive manufacturing process begins. This preliminary action removes oxygen and contaminants from the environment beforehand, preventing contamination during printing without requiring continuous complex purification systems throughout the entire process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent implements an inert atmosphere environment using high-purity argon or helium gas (99.995% or higher purity) to surround the molten pool and powder during the additive manufacturing process. This inert environment prevents oxidation and contamination of the metal powder and deposited material, directly improving product quality and mechanical properties without requiring complex in-situ purification systems.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

2Object-affected harmful factors

If dynamic gas flowrate adjustment using sensors is implemented, then contaminant removal is improved, but device complexity increases

Engineering Contradiction:
Improvecontaminant removalVSAvoiddevice complexity
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

The system incorporates oxygen sensors that continuously monitor the oxygen concentration in the printing chamber and powder feed system. Based on the sensor readings, the gas flowrate is dynamically adjusted in real-time to maintain optimal oxygen levels. This feedback mechanism efficiently removes contaminants by increasing gas flow when contamination is detected, while avoiding unnecessary high flow rates when the environment is already clean, thus balancing contaminant removal with system simplicity.

Inventive Principle:
Principle #23Feedback

3Manufacturing precision

If high purity inert gas is used throughout the process, then oxide inclusions and porosity are reduced, but gas consumption and cost increase

Engineering Contradiction:
Improveoxide inclusions and porosity reductionVSAvoidgas consumption
Core Design Contradiction:
Manufacturing precisionVSQuantity of substance

Solution Approach 1:

The system uses high-purity inert gas for purging the printing chamber and powder feed system before the additive manufacturing process begins. This preliminary purging action establishes a clean inert environment beforehand, allowing the actual printing process to proceed with reduced gas consumption while still maintaining low oxide inclusion and porosity levels in the final product.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent applies high-purity inert gas selectively to critical areas and times during the process - specifically during purging operations and when oxygen sensors detect elevated contaminant levels. Rather than maintaining maximum gas flow continuously, the system uses partial action (reduced flow) during stable clean conditions, thereby reducing overall gas consumption while still achieving the goal of minimizing oxide inclusions and porosity in the printed parts.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly improves product quality by reducing contaminant effects, enhancing mechanical properties, and increasing productivity by creating a controlled environment that minimizes oxide inclusions, porosity, and surface defects, potentially reducing the need for post-processing treatments like HIP.

Implementation Method 1

a sweep stream of an ultra-pure Ar or He, can facilitate the removal of these contaminants

Methodology Applied
Scientific EffectPurging:

Implementation Method 2

laser 3-dimensional printing (3DP) of metallic parts

Methodology Applied
Scientific EffectLaser heating: Laser

Implementation Method 3

When these powders are re-melted during typical 3DP operations

Methodology Applied
Scientific EffectMelting: Melting

Implementation Method 4

providing one or more gas sensors located in one or more of the printing chamber, gas supply system, or feed powder systems

Methodology Applied
Scientific EffectGas sensing:

Data Source

PatentUS10730142B2Gas atmosphere control in laser printing using metallic powders
Publication Date: 2020.08.04 AIR PROD & CHEM INC
  • US10730142B2 patent drawing
  • US10730142B2 patent drawing

AI summary

Methods and systems for controlling gas atmospheres in three-dimensional laser printing and weld overlay consolidation operations using metallic powders are provided. In one or more embodiments, such systems and methods comprise a printing chamber or laser weld overlay system, a gas supply system, a feed powder system, and one or more sensors employed to control the printing or welding operation. The methods and systems of the invention employ one or more inert gases having a purity greater than or equal to 99.995%