Inert Gas Plasma Coating at Atmospheric Pressure for Adhesion Control

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Solution Overview

Problem

Existing plasma coating techniques fail to alter adhesion properties in a controlled manner, particularly due to the use of reactive gases that lead to uncontrolled reactions and loss of adhesion property control, and they are limited by the need for vacuum conditions and the inability to handle a wide range of substrates and precursors.

Innovation Solution

A method using an inert gas plasma at atmospheric pressure with low temperature and minimal reactive gas content, allowing controlled alteration of adhesion properties by introducing a precursor in a plasma afterglow, which avoids direct exposure to plasma zones and electromagnetic fields, enabling treatment of various substrates and precursors.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If reactive gases are used in plasma coating to enable coating formation, then coating deposition is achieved, but adhesion property control is lost due to uncontrolled reactions

Engineering Contradiction:
Improveadhesion property controlVSAvoiduncontrolled chemical reactions
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

The patent uses an inert gas atmosphere (nitrogen or nitrogen-containing gas) as the plasma environment instead of reactive gases. This inert atmosphere prevents uncontrolled chemical reactions between the plasma and precursor molecules, thereby maintaining precise control over adhesion properties while still enabling coating formation through physical deposition and controlled surface interaction.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

2Manufacturing precision

If vacuum plasma techniques are used to achieve controlled coating, then coating quality is improved, but processing time increases due to depressurizing steps

Engineering Contradiction:
Improvecoating qualityVSAvoidprocessing time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The patent changes the pressure parameter from vacuum conditions to atmospheric pressure operation. By using nitrogen plasma at atmospheric pressure, the process eliminates time-consuming vacuum depressurization and pressurization steps while maintaining controlled coating quality through the inert atmosphere that prevents unwanted reactions.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If wet coating techniques are used to apply coating material, then coating application is simplified, but drying time increases and environmental stress increases

Engineering Contradiction:
Improvecoating application simplicityVSAvoiddrying time
Core Design Contradiction:
Ease of manufactureVSLoss of time

Solution Approach 1:

The patent replaces wet coating techniques (liquid application followed by drying) with plasma-enhanced physical vapor deposition. The coating material is deposited in a nitrogen plasma environment, forming a coating directly without requiring subsequent drying steps, thereby eliminating both drying time and environmental waste issues associated with solvent evaporation.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

4Strength

If high temperature plasma is used to activate surface, then adhesion enhancement is achieved, but substrate damage occurs due to thermal stress

Engineering Contradiction:
Improveadhesion strengthVSAvoidthermal damage to substrate
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The patent employs nitrogen plasma at atmospheric pressure, which operates at lower temperatures compared to vacuum plasma techniques. The inert nitrogen atmosphere enables surface activation and coating formation without requiring high temperatures, thereby enhancing adhesion strength while avoiding thermal damage to temperature-sensitive substrates.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method achieves precise control over adhesion properties, allowing both increased and decreased adhesion as needed, with coatings that are durable, homogeneous, and conformal, suitable for a wide range of materials without the drawbacks of traditional methods.

Implementation Method 1

ionizing a plasma gas at low temperature and at atmospheric pressure, thereby creating a plasma

Methodology Applied
Scientific EffectPlasma: Plasma

Implementation Method 2

a substrate film or web is coated by vapor deposition of the vaporized substance at atmospheric pressure in the plasma field

Methodology Applied
Scientific EffectVapor deposition: Physical Vapour Deposition

Data Source

PatentUS12503624B2Method for altering adhesion properties of a surface by plasma coating
Publication Date: 2025.12.23 MOLECULAR PLASMA GRP SA
  • US12503624B2 patent drawing
  • US12503624B2 patent drawing
  • US12503624B2 patent drawing

AI summary

A method for altering adhesion properties of a surface of a substrate by a coating, comprising the steps of: a) ionizing a plasma gas at low temperature and at atmospheric pressure, thereby creating a plasma with a plasma temperature of at most 50° C.; b) introducing a precursor into a plasma gas afterglow of the plasma; c) subjecting the surface of the substrate to the plasma including the precursor, thereby forming a coating onto the surface. The plasma gas is essentially completely comprised of inert gas. The coating alters the adhesion properties of the surface.