InGaAs/InP Photodetector Fabrication With Selective Phosphorus Removal

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Solution Overview

Problem

In the production of light-receiving devices using InGaAs/InP-based materials, phosphorus precipitates on the wafer surface after impurity diffusion treatment, leading to reduced light-receiving sensitivity and increased ohmic resistance, necessitating a method for selective removal of these precipitates without etching the underlying InP and InGaAs layers.

Innovation Solution

A method involving the sequential growth of an InP buffer layer, an InGaAs light absorption layer, and an InP cap layer on an InP substrate, followed by forming an InGaAs contact layer, removing part of it, and diffusing impurities in a phosphorus-containing atmosphere. The method includes selectively removing phosphorus precipitates using a strong aqueous base, such as TMAH, to minimize etching of InP and InGaAs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a rapid temperature falling rate is used during impurity diffusion treatment, then excessive diffusion is prevented and manufacturing efficiency is improved, but phosphorus precipitates form on the wafer surface which degrades light-receiving characteristics and increases ohmic resistance

Engineering Contradiction:
Improvemanufacturing efficiencyVSAvoidlight-receiving characteristics
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

A protective film is formed on the wafer surface before impurity diffusion treatment to prevent phosphorus precipitation. This preliminary protective measure allows rapid cooling to be used without the harmful side effect of phosphorus precipitate formation, thus resolving the contradiction between manufacturing efficiency and device reliability

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent converts the harmful phosphorus precipitation phenomenon into a removable surface layer by forming a specific protective film structure that incorporates phosphorus in a controllable manner. The protective film is then selectively removed to reveal a clean surface, transforming the potential harm into a controlled process step

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Productivity

If a rapid temperature falling rate is used during impurity diffusion treatment, then excessive diffusion is prevented, but phosphorus precipitates form on the wafer surface which increases ohmic resistance during electrode formation

Engineering Contradiction:
Improvediffusion process efficiencyVSAvoidohmic resistance
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The protective film is formed in advance before diffusion treatment to prevent phosphorus precipitation that would later cause high ohmic resistance. This allows the diffusion process to proceed efficiently with rapid cooling without generating the harmful precipitates

Inventive Principle:
Principle #10Preliminary action

3Reliability

If phosphorus precipitates are removed by etching, then light-receiving characteristics are improved, but InP and InGaAs layers are also etched which damages the wafer structure

Engineering Contradiction:
Improvelight-receiving characteristicsVSAvoidwafer structure integrity
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The protective film is selectively removed (taken out) from the wafer surface after diffusion treatment, extracting only the phosphorus-containing protective layer while leaving the underlying InP and InGaAs layers intact. This selective removal eliminates phosphorus precipitates without damaging the sensitive semiconductor structure

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The protective film acts as an intermediary layer that can be selectively removed using specific etchants that do not attack the InP and InGaAs layers. This intermediary structure enables selective phosphorus removal while protecting the underlying wafer structure from etching damage

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method allows for the selective removal of phosphorus precipitates, thereby improving the light-receiving characteristics and reducing ohmic resistance in the light-receiving device, while maintaining the integrity of the InP and InGaAs layers.

Implementation Method 1

selectively removing a phosphorus precipitate adhered to a surface in the step of diffusing the impurity using a strong aqueous base

Methodology Applied
Scientific EffectSelective etching:

Implementation Method 2

diffusing an impurity to the opening pattern portion in a phosphorus-containing atmosphere

Methodology Applied
Scientific EffectDiffusion: Diffusion

Implementation Method 3

using an epitaxial wafer in which an InP buffer layer, an InGaAs light absorption layer, and an InP cap layer are epitaxially grown sequentially on an InP substrate

Methodology Applied
Scientific EffectEpitaxial growth: Epitaxy

Data Source

PatentEP4546434A1Method for manufacturing light-receiving element
Publication Date: 2025.04.30 SHIN ETSU HANDOTAI CO LTD
  • EP4546434A1 patent drawingFigure 1~2
  • EP4546434A1 patent drawingFigure 3~4
  • EP4546434A1 patent drawingFigure 5~6

AI summary

The present invention is a method for producing a light-receiving device using an epitaxial wafer in which an InP buffer layer, an InGaAs light absorption layer, and an InP cap layer are grown on an InP substrate, the method including the steps of forming an InGaAs contact layer on the InP cap layer, removing a part of the InGaAs contact layer by a photolithography method to form an InGaAs contact portion, forming a protective film so as to coat the InP cap layer and the InGaAs contact portion, forming an opening pattern portion in a part of the protective film, diffusing an impurity to the opening pattern portion in a phosphorus-containing atmosphere, selectively removing a phosphorus precipitate adhered to a surface in the step of diffusing the impurity using a strong aqueous base, and forming an electrode on the InGaAs contact portion and a back surface of the InP substrate. This provides the method for producing a light-receiving device, in which only a phosphorus precipitate precipitated on a wafer surface can be selectively removed.