Dry Powder Inhaler Particle Size Control

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Solution Overview

Problem

Inhalable β2-agonists used for treating respiratory diseases often cause cardiac side effects due to systemic exposure, and combination products with corticosteroids complicate dose control, particularly for β2-agonists with narrower therapeutic windows.

Innovation Solution

A dry powder inhaler with a cyclone deagglomerator and a β2-agonist formulation having a narrowly defined particle size distribution, specifically d90 values between 3.5-6 microns, reduces systemic exposure and minimizes cardiac side effects, using jet milling to produce particles with controlled size and a lactose carrier for effective lung deposition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If β2-agonists are administered via inhalation to treat respiratory diseases, then therapeutic effect is achieved, but cardiac side effects occur due to systemic exposure

Engineering Contradiction:
Improvetherapeutic effectVSAvoidcardiac side effects
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent changes the particle size parameter of the β2-agonist from conventional fine micronisation (d90 < 3.5 µm) to a coarser distribution (d90 = 3.5-6 µm). This parameter change reduces systemic absorption and cardiac side effects while maintaining pulmonary therapeutic efficacy through optimized lung deposition characteristics

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a localized effect by optimizing particle size for lung-specific deposition. The coarser particle size distribution ensures particles deposit primarily in the lungs where they are needed, reducing systemic exposure and cardiac side effects while maintaining local therapeutic concentration

Inventive Principle:
Principle #3Local quality

2Ease of operation

If particles are micronised to small size (1-5 microns) for lung inhalation, then delivery to lungs is effective, but particles deposit in throat and are swallowed causing systemic exposure

Engineering Contradiction:
Improveinhalation deliveryVSAvoidsystemic exposure
Core Design Contradiction:
Ease of operationVSLoss of substance

Solution Approach 1:

The patent modifies the particle size parameter from fine micronisation (1-5 µm) to a coarser distribution (d90 = 3.5-6 µm). This change reduces throat deposition and swallowing, thereby minimizing systemic exposure while maintaining effective lung delivery through optimized aerodynamic properties

Inventive Principle:
Principle #35Parameter changes

3Ease of operation

If combination products are used to improve patient convenience and compliance, then patient compliance improves, but control over individual dose is reduced

Engineering Contradiction:
Improvepatient complianceVSAvoiddose control
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The patent segments the combination product into separate dosage forms or separate actuation mechanisms for each active ingredient. This allows independent dosing control of the β2-agonist and corticosteroid while maintaining the convenience of a single inhaler device, enabling precise control over the β2-agonist dose to avoid exceeding the narrow therapeutic window

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution significantly reduces systemic exposure to β2-agonists, minimizing cardiac side effects and ensuring effective delivery to the lungs while maintaining therapeutic efficacy, as demonstrated by reduced Cmax in pharmacokinetic studies.

Implementation Method 1

The particle size of the β2-agonist powder is measured by laser diffraction as a dry dispersion, e.g. in air, such as with a Sympatec HELOS/BF equipped with a RODOS disperser

Methodology Applied
Scientific EffectJet milling: Jet Erosion

Implementation Method 2

a cyclone deagglomerator for breaking up agglomerates of the dry powder medicament

Methodology Applied
Scientific EffectCyclone separation: Cyclone Separation

Implementation Method 3

The particle size of the β2-agonist powder is measured by laser diffraction as a dry dispersion

Methodology Applied
Scientific EffectLaser diffraction: Diffraction

Data Source

PatentEP3590499B1Inhalable medicaments
Publication Date: 2022.10.05 PHARMACHEMIE BV
  • EP3590499B1 patent drawingFigure 1
  • EP3590499B1 patent drawingFigure 2
  • EP3590499B1 patent drawingFigure 3

AI summary

The present invention provides a dry powder inhaler comprising: a reservoir containing a dry powder formulation and an arrangement for delivering a metered dose of the medicament from the reservoir; and a delivery passageway for directing an inhalation-induced air flow through a mouthpiece, the delivery passageway extending to the metered dose of medicament, wherein the formulation comprises an inhalable β2-agonist having a particle size distribution of d10 &lt;1 µm, d50 = 1-3 µm, d90 = 3.5-6 µm and NLT 99% &lt;10 µm and a lactose carrier.