Ink Set Discharge Stability via Reaction Liquid Extraction

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Solution Overview

Problem

Conventional aqueous inks for ink-jet printing face issues with discharge stability and film formation on non-absorbing or low-absorbing substrates, leading to beading, unevenness, and poor adherence due to the presence of film-forming aids in the ink, which can cause nozzle clogging and inadequate film strength.

Innovation Solution

Incorporating a glycol ether-based solvent and/or glycol ether acetate-based solvent in the reaction liquid instead of the aqueous ink, with an emulsion glass transition temperature set at 50° C. or higher, improves discharge stability and film properties such as rubbing resistance and adherence.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If film-forming aids (glycol ether-based solvent, glycol ether acetate-based solvent) are contained in the aqueous ink, then film formability and rubbing resistance are improved, but nozzle clogging occurs and discharge stability deteriorates

Engineering Contradiction:
Improvefilm strengthVSAvoiddischarge stability
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent extracts the film-forming aid (glycol ether-based solvent and/or glycol ether acetate-based solvent) from the aqueous ink formulation and places it only in the reaction liquid. This separation eliminates the harmful effect of film-forming aids causing nozzle clogging while preserving their beneficial film-forming properties in the reaction liquid where they contribute to coating film formation without compromising discharge stability.

Inventive Principle:
Principle #2Taking out (Extraction)

2Ease of manufacture

If emulsion glass transition temperature is set low for easy film formation, then film formation at ambient temperature is facilitated, but nozzle clogging occurs due to emulsion solidification

Engineering Contradiction:
Improvefilm formation easeVSAvoiddischarge stability
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent changes the glass transition temperature parameter of the emulsion to 50°C or higher, which prevents emulsion solidification at nozzle temperatures and ensures stable discharge. Simultaneously, the reaction liquid containing glycol ether-based solvent and/or glycol ether acetate-based solvent enables the emulsion to form films with adequate adherence and rubbing resistance despite the higher glass transition temperature.

Inventive Principle:
Principle #35Parameter changes

3Adaptability or versatility

If conventional aqueous ink is used on non-absorbing or low-absorbing substrates, then substrate compatibility is achieved, but drying speed decreases and beading occurs

Engineering Contradiction:
Improvesubstrate compatibilityVSAvoiddrying speed
Core Design Contradiction:
Adaptability or versatilityVSSpeed

Solution Approach 1:

The patent segments the ink system into two separate components: aqueous ink for substrate coverage and reaction liquid for film formation. The reaction liquid, containing aggregating agent and film-forming aids, is discharged simultaneously or sequentially to promote rapid drying and prevent beading on non-absorbing or low-absorbing substrates while maintaining substrate compatibility through the aqueous ink component.

Inventive Principle:
Principle #1Segmentation

4Productivity

If aqueous ink is discharged with short interval on non-absorbing substrate, then printing efficiency is improved, but inter-color bleeding occurs due to insufficient drying

Engineering Contradiction:
Improveprinting efficiencyVSAvoidimage quality
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by including the reaction liquid with aggregating agent and film-forming aids that promote rapid drying and film formation. This preliminary preparation in the reaction liquid formulation enables the ink to dry quickly even when discharged with short intervals, preventing inter-color bleeding and maintaining image quality while allowing high printing efficiency.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed ink set achieves enhanced discharge stability and improved coated film properties, including better rubbing resistance and adherence, while preventing nozzle clogging and ensuring sufficient film strength.

Implementation Method 1

an emulsion contained in an aqueous ink becomes easier to form a film by drying at an ambient temperature

Methodology Applied
Scientific EffectDrying: Evaporation

Implementation Method 2

By containing the film-forming aid of the aqueous ink, an emulsion contained in an image formed on the surface of a recording medium sufficiently sticks thereto to form a film

Methodology Applied
Scientific EffectFilm formation:

Implementation Method 3

an image is formed by volatilization of a solvent such as water and an organic solvent contained in the aqueous ink, on the surface of a recording medium

Methodology Applied
Scientific EffectVolatilization: Evaporation

Data Source

PatentUS10676631B2Ink set for ink-jet printing and ink-jet recording method
Publication Date: 2020.06.09 MAXELL LTD

AI summary

There is provided an ink set for ink-jet printing comprising an aqueous ink and a reaction liquid, wherein the aqueous ink contains an emulsion, a surfactant, an organic solvent, a pigment, and water, the reaction liquid contains an aggregating agent, 1,2-alkanediol, a glycol ether-based solvent and/or a glycol ether acetate-based solvent, and water, and the emulsion has a glass transition temperature of 50° C. or higher. The ink set for ink-jet printing is provided with an aqueous ink excellent in the discharge stability, and can form an image excellent in coated film properties such as the rubbing resistance and the adherence.