Ink Jet Printing Method for Titanium Oxide Precipitation Control

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Solution Overview

Problem

Inkjet printing methods face challenges with the precipitation of titanium oxide in white inks, leading to instability in ink discharge and image unevenness, particularly on transparent or low-absorbency print media.

Innovation Solution

The method involves enhancing the redispersibility of titanium oxide particles by maintaining a circulation flow rate within the liquid discharge head that exceeds the precipitation velocity, ensuring uniform pigment concentration and stable discharge through a mechanism that promotes redispersion within the circulation path.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Illumination intensity

If titanium oxide is used as a colorant in white ink, then whiteness and concealability are improved, but precipitation occurs leading to discharge instability and image unevenness

Engineering Contradiction:
ImprovewhitenessVSAvoiddischarge stability
Core Design Contradiction:
Illumination intensityVSReliability

Solution Approach 1:

The invention changes the surface treatment parameters of titanium oxide particles by applying specific surface treatments (silane coupling agent treatment, alumina treatment, or combination treatments) with controlled treatment conditions and sequences. This modifies the surface properties to enhance redispersibility while maintaining the whitening effect, thereby resolving the contradiction between whiteness and discharge stability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates composite structures on titanium oxide particles by combining multiple surface treatments (silane coupling agents with alumina, or dual silane coupling agents). These composite surface treatments provide both the whitening properties of titanium oxide and the dispersibility enhancement from multiple functional layers, resolving the contradiction between concealability and discharge stability.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If titanium oxide particles are dispersed in white ink, then concealability is improved, but particles precipitate over time causing image unevenness

Engineering Contradiction:
Improvepigment concentrationVSAvoiddispersion stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The invention modifies the surface parameters of titanium oxide particles through controlled surface treatments that change the surface charge, hydrophilicity, and steric hindrance properties. These parameter changes enhance the colloidal stability of the pigment suspension, allowing high pigment concentration to be maintained with improved dispersion stability and reduced precipitation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention introduces surface treatment agents (silane coupling agents, alumina) as intermediaries between the titanium oxide particles and the ink medium. These intermediaries improve the compatibility between pigment particles and the liquid carrier, preventing aggregation and precipitation while maintaining high pigment concentration for better concealability.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If circulation flow rate is increased to prevent precipitation, then discharge stability is improved, but energy consumption increases

Engineering Contradiction:
Improvedischarge stabilityVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The invention changes the rheological parameters of the ink by modifying particle surface properties, which reduces the viscosity and improves flow characteristics. This allows the system to maintain discharge stability with lower circulation flow rates, thereby reducing energy consumption while preventing precipitation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention performs preliminary surface treatment of titanium oxide particles to enhance their redispersibility before ink formulation. This preliminary action creates particles that resist aggregation and precipitation, reducing the need for high-energy circulation systems and lowering ongoing energy consumption while maintaining discharge stability.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach improves the discharge stability of inks containing titanium oxide, preventing precipitation and maintaining image quality by ensuring consistent ink flow and pigment distribution.

Implementation Method 1

titanium oxide has a problem of easily precipitating

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Implementation Method 2

using a titanium oxide particle having high redispersibility

Methodology Applied
Scientific EffectRedispersibility: Dispersion (of waves)

Data Source

PatentEP4477421A1Ink jet printing method
Publication Date: 2024.12.18 CANON KK
  • EP4477421A1 patent drawingFigure 1A~1B
  • EP4477421A1 patent drawingFigure 2
  • EP4477421A1 patent drawingFigure 3A~3B

AI summary

In an ink jet printing method for discharging ink from a liquid discharge head (1), the ink contains titanium oxide having a precipitation velocity of 1.0×10-11 m/s or more based on a Stokes equation in the ink, the liquid discharge head (1) comprises a discharge port (13), a pressure chamber (12), an energy-generating element for discharging the ink, an upstream flow channel for supplying a liquid to the pressure chamber (12), a downstream flow channel communicating with the pressure chamber (12), and a pump communicating with the upstream and downstream flow channels and forming a circulation path in which the ink circulates in an order of the upstream flow channel, pressure chamber (12), downstream and upstream flow channels, and a ratio of the flow rate Q of the ink to the maximum cross-sectional area S of the circulation path, Q/S [m/s], is higher than the precipitation velocity.