Inline Buffer Dilution With Backpressure-Controlled Mixing

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Solution Overview

Problem

Existing inline buffer dilution systems face challenges in maintaining consistent mixing quality across varying fluid flows, particularly in ensuring adequate mixing at different flow rates, which limits their scalability and efficiency in producing solutions with desired characteristics like pH, conductivity, and refractive index.

Innovation Solution

The inline buffer dilution system employs a scalable design with proportional pinch valves, a programmable logic controller, and a mixing pump with adjustable backpressure, ensuring consistent mixing across a range of fluid flows by controlling the flow of diluent and buffer liquids and using sensors for real-time feedback to maintain desired solution characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If external pressurization is used to maintain buffer flow, then fluid flow is improved, but device complexity and cost increase

Engineering Contradiction:
Improvefluid flow rateVSAvoidpressurization system complexity
Core Design Contradiction:
SpeedVSDevice complexity

Solution Approach 1:

The system uses the peristaltic pump's inherent pumping action to create negative pressure that draws buffer solution through the mixing chamber, eliminating the need for external pressurization devices. The pump itself provides both the driving force for fluid flow and the mixing action through its rotating rollers compressing the tubing.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent removes the external pressurization system from the overall design, using only the pump's internal mechanisms to achieve both fluid delivery and mixing functions. This extraction of unnecessary components simplifies the device while maintaining functionality.

Inventive Principle:
Principle #2Taking out (Extraction)

2Manufacturing precision

If mixing chamber volume is increased to improve mixing quality, then mixing effectiveness is improved, but device size and fluid residence time increase

Engineering Contradiction:
Improvemixing qualityVSAvoidmixing chamber volume
Core Design Contradiction:
Manufacturing precisionVSVolume of moving object

Solution Approach 1:

The peristaltic pump creates pulsating flow and mechanical compression of the tubing as it rotates, generating turbulent mixing effects within a compact chamber. The periodic compression and release of tubing by the pump rollers creates shear forces that enhance mixing without requiring a large chamber volume.

Inventive Principle:
Principle #18Mechanical vibration

Solution Approach 2:

The system uses fluid dynamics and pressure variations created by the peristaltic pumping action to achieve effective mixing. The alternating compression and decompression of the fluid stream within the narrow chamber creates sufficient turbulence for thorough mixing of buffer solutions.

Inventive Principle:
Principle #29Pneumatics and hydraulics

3Productivity

If flow rate is increased to improve productivity, then output is improved, but mixing quality deteriorates

Engineering Contradiction:
Improvesolution production rateVSAvoidmixing consistency
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The peristaltic pump provides dynamic mixing through its rotating motion, where the speed and pattern of roller compression can be adjusted to maintain effective mixing across a range of flow rates. The system adapts the mixing mechanism to the flow conditions, allowing high productivity while preserving mixing quality.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The buffer solutions are pre-mixed in their respective reservoirs before entering the mixing chamber, ensuring homogeneous input streams. This preliminary preparation allows the compact mixing chamber to achieve final blending efficiency even at higher flow rates.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration ensures a minimum mixing threshold across a range of fluid flows from 2 to 20 liters per minute, allowing for the production of solutions with precise characteristics, such as pH and conductivity, while reducing the need for external pressurization of buffer solutions and enabling the use of disposable containers.

Implementation Method 1

a peristaltic mixing pump downstream of the flow control valves

Methodology Applied
Scientific EffectPeristalsis: Peristalsis

Implementation Method 2

a conductivity sensor and a pH sensor downstream of the mixing pump

Methodology Applied
Scientific EffectElectrical conductivity measurement: Conduction (electrical)

Implementation Method 3

a conductivity sensor and a pH sensor downstream of the mixing pump

Methodology Applied
Scientific EffectpH measurement:

Data Source

PatentEP4081877B1Scaleable inline buffer dilution scheme
Publication Date: 2024.01.10 ASAHI KASEI BIOPROCESS AMERICA INC
  • EP4081877B1 patent drawingFigure 1
  • EP4081877B1 patent drawingFigure 2~3

AI summary

An inline buffer dilution system is provided that includes a first flow control valve fluidly connected to a supply of diluent liquid, second and third flow control valves fluidly connected to supplies of a first buffer and a second buffer, respectively, and a mixing pump fluidly connected to the first, second, and third flow control valves and configured to mix an amount of the diluent liquid, the first buffer, and the second buffer to produce a diluted buffer solution. The system further includes a backpressure control valve configured to generate a backpressure that promotes mixing within the mixing pump, and a controller configured to control the backpressure based on the amount of the diluent liquid, the first buffer, and the second buffer being mixed in the mixing pump, such that the mixing pump yields a minimum mixing threshold across a range of fluid flows.