Insulated chamber and method for flushing such a chamber

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Solution Overview

Problem

Existing insulated chambers used in air separation units, particularly those employing solid insulation at subambient or cryogenic temperatures, face inefficiencies in nitrogen distribution, leading to inadequate thermal performance, risk of moisture ingress, and potential ignition hazards due to uneven gas flow and incomplete flushing.

Innovation Solution

The implementation of a nitrogen flushing system that injects gas containing at least 95% nitrogen into the insulation via vertically positioned, perforated pipes or porous flexible pipes, ensuring even distribution across the chamber, particularly above insulated elements, to maintain a dry atmosphere and prevent condensation and ignition risks.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If nitrogen is sent through an opening in the roof of the chamber, then the nitrogen passes freely through the insulation, but the distribution of nitrogen is not good

Engineering Contradiction:
Improvenitrogen distributionVSAvoiddistribution system
Core Design Contradiction:
Ease of operationVSDevice complexity

Solution Approach 1:

The distribution system is segmented into multiple injection points positioned at different locations (roof, walls, bottom) of the chamber. This segmentation allows nitrogen to be injected at multiple strategic positions, creating a more uniform distribution pattern throughout the insulation rather than relying on a single opening.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different regions of the chamber are provided with different injection characteristics. The roof opening provides top-down flow, wall injections provide lateral distribution, and bottom injections provide upward flow. Each location is optimized for its specific position to achieve overall uniform distribution.

Inventive Principle:
Principle #3Local quality

2Ease of operation

If gaseous nitrogen is sent from the distillation into the insulation by means of a distributer positioned in the middle of the mass of insulation, then nitrogen is injected centrally, but optimal distribution of the inert gas is not achieved

Engineering Contradiction:
Improvegas distributionVSAvoiddistribution uniformity
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The single central distributer is replaced by multiple injection points distributed throughout the chamber structure (roof, walls, bottom). This segmentation eliminates the concentration of flow at one location and enables nitrogen to reach all regions of the insulation more uniformly.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The injection system transitions from a single-point (0D) or localized (2D) distribution to a three-dimensional distribution network. Injection points are positioned at roof, walls, and bottom, creating volumetric coverage that ensures uniform gas distribution throughout the entire insulation mass.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

3Reliability

If nitrogen is used to maintain a dry atmosphere with slight overpressure, then moisture ingress is prevented, but the thermal performance of the insulation is impaired if moisture enters

Engineering Contradiction:
Improvemoisture protectionVSAvoidthermal performance
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

Nitrogen injection is implemented as a preliminary and continuous protective action before and during any potential moisture ingress scenarios. By maintaining continuous nitrogen flow and positive pressure, the system proactively prevents moisture entry rather than reacting after contamination occurs.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

An inert nitrogen atmosphere is established and maintained within the insulation chamber. This inert environment prevents both moisture ingress and oxygen-related safety hazards, creating a protective atmosphere that preserves insulation thermal performance and ensures operational safety.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

4Object-affected harmful factors

If air enters the insulation, then oxygen-enriched air may condense below the dew point, but the risk of ignition and explosion increases

Engineering Contradiction:
Improvecondensation riskVSAvoidignition risk
Core Design Contradiction:
Object-affected harmful factorsVSObject-generated harmful factors

Solution Approach 1:

Nitrogen injection creates and maintains an inert atmosphere within the insulation, replacing oxygen-containing air with nitrogen. This eliminates the risk of oxygen-enriched air condensation and removes the ignition hazard entirely, as nitrogen is non-flammable and displaces oxygen needed for combustion.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Solution Approach 2:

The system applies preliminary anti-action by continuously injecting nitrogen to prevent the formation of flammable or oxygen-enriched conditions before they can occur. The inerting action counteracts any potential air ingress that could lead to condensation or ignition hazards.

Inventive Principle:
Principle #9Preliminary anti-action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution enhances nitrogen distribution within the insulated chamber, improving thermal performance, reducing the risk of moisture ingress and ignition, while simplifying installation and reducing costs by using less expensive and lighter porous pipes, ensuring comprehensive flushing and efficient operation.

Implementation Method 1

at least some of the means for injecting the gas into the insulation open into the insulation arranged at a position vertically above at least one element that is to be insulated, so that the gas can seep out

Methodology Applied
Scientific EffectGas seepage through porous material: Permeation

Data Source

PatentUS10920935B2Insulated chamber and method for flushing such a chamber
Publication Date: 2021.02.16 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • US10920935B2 patent drawing
  • US10920935B2 patent drawing

AI summary

The invention relates to an insulated chamber comprising at least one element that may operate at sub-ambient temperature, the space around the element(s) being filled with solid insulation and means for injecting a gas containing at least 95 mol-% nitrogen into the insulation, at least some of the gas-injection means opening at a position vertically above at least one element to insulate.