Radiation Curable Intaglio Ink Stability and Wipeability

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Solution Overview

Problem

Radiation curable intaglio inks for security documents face challenges with stability upon storage and use, optimized rheology, good wipeability, and detergeability in standard alkaline aqueous wiping solutions, as existing inks suffer from poor pot life, surface skin formation, and instability on printing presses.

Innovation Solution

A radiation curable intaglio ink composition comprising 10-60 wt% radiation curable compounds, 2-20 wt% photoinitiators, 5-12 wt% high molecular weight acid modified alkyd or alkylarene sulfonic acid surfactants, and 10-55 wt% fillers, with specific viscosity and surfactant properties, optimized for UV-Vis curing and alkaline aqueous cleaning.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If radiation curable compounds are used in intaglio ink, then rapid curing and high production rates are achieved, but stability upon storage and surface skin formation occur

Engineering Contradiction:
Improveproduction rateVSAvoidstorage stability
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

The patent modifies the chemical parameters of the radiation curable compounds by selecting specific types (epoxy acrylates, polyester acrylates, urethane acrylates) and controlling their molecular weight and functionality. It also adjusts the photoinitiator system composition and concentration to optimize both storage stability and curing performance, resolving the contradiction between rapid curing and storage stability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite ink formulation combining multiple radiation curable compounds with different chemical structures, photoinitiators, resins, and additives. This composite approach allows the ink to maintain stability during storage while enabling complete and uniform curing during printing, thus resolving the contradiction between storage stability and production rate

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If intaglio printing process is used, then high quality fine line printing and relief features are achieved, but massive quantities of ink-impregnated waste are generated

Engineering Contradiction:
Improveprinting qualityVSAvoidwaste generation
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The patent employs oxidative polymerization mechanism where oxygen from air acts as a crosslinking agent during drying. This oxidation process allows the ink to cure completely without requiring excessive ink removal, reducing waste while maintaining the characteristic intaglio relief and fine line quality

Inventive Principle:
Principle #38Strong oxidants (Accelerated oxidation)

Solution Approach 2:

The patent replaces the traditional mechanical wiping system with a chemical curing system. Instead of relying on physical removal of excess ink through wiping cylinders, the ink chemically cures in place, eliminating the need for massive waste removal while preserving the intaglio printing quality

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Productivity

If polymeric wiping cylinder is used to remove ink excess, then printing speed is maintained, but cleaning of the wiping cylinder becomes problematic

Engineering Contradiction:
Improveprinting speedVSAvoidwiping cylinder cleaning
Core Design Contradiction:
ProductivityVSEase of manufacture

Solution Approach 1:

The radiation curable ink formulation is designed to cure rapidly upon exposure to UV or visible light, allowing the wiping cylinder to self-clean as the cured ink adheres to the substrate rather than sticking to the wiping surface. This eliminates the need for complex cleaning systems while maintaining high printing speeds

Inventive Principle:
Principle #25Self-service

4Stability of the object's composition

If conventional oxidative drying is used, then ink stability is maintained, but drying time is extended and set-off occurs

Engineering Contradiction:
Improveink stabilityVSAvoiddrying time
Core Design Contradiction:
Stability of the object's compositionVSLoss of time

Solution Approach 1:

The patent incorporates photoinitiators and oxidation catalysts in the ink formulation that are activated by UV or visible light exposure during printing. This preliminary activation triggers rapid polymerization and crosslinking, eliminating the need for extended oxidative drying time while preventing set-off, thus resolving the contradiction between ink stability and drying time

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The ink exhibits improved stability, rapid curing, enhanced wipeability, and effective detergeability, ensuring high production rates and reduced set-off issues, while maintaining security features as patterns or images on substrates.

Implementation Method 1

radiation curable compounds, wherein at least one of said one or more radiation curable compounds is a fatty acid polyester (meth)acrylate oligomer

Methodology Applied
Scientific EffectPhotopolymerisation: Photopolymerisation

Implementation Method 2

from about 2 wt-% to about 20 wt-% of one or more photoinitiators

Methodology Applied
Scientific EffectAbsorption (EM radiation): Absorption (EM radiation)

Implementation Method 3

from about 5 wt-% to about 12 wt-% of a high molecular weight acid modified alkyd surfactant and/or an alkylarene sulfonic acid surfactant

Methodology Applied
Scientific EffectSurfactant: Surfactant

Implementation Method 4

enhanced wipeability

Methodology Applied
Scientific EffectWetting: Wetting

Implementation Method 5

Wiping off using an aqueous solution as an emulsifying medium for the wiped-off excess ink

Methodology Applied
Scientific EffectEmulsion: Emulsion

Implementation Method 6

effective detergeability

Methodology Applied
Scientific EffectClean:

Data Source

PatentEP4004130B1Radiation curable intaglio inks
Publication Date: 2023.06.14 SICPA HOLDING SA
  • EP4004130B1 patent drawingFigure 1A~1B

AI summary

The present invention relates to the field of security documents and their protection against counterfeit and illegal reproduction and relates to the field of intaglio printing processes for the printing of said security documents. In particular, the present invention relates to radiation curable intaglio inks suitable for intaglio printing a pattern or image, wherein said intaglio printing comprises wiping off ink excess with a polymeric wiping cylinder and cleaning said cylinder with an alkaline aqueous wiping solution. The disclosed radiation curable intaglio inks comprise one or more radiation curable compounds, wherein at least one of said one or more radiation curable compounds is a fatty acid polyester (meth)acrylate oligomer; one or more photoinitiators; and a high molecular weight acid modified alkyd surfactant and/or an alkylarene sulfonic acid surfactant; one or more fillers or extenders.