Integrating Sphere Light Collector for Biological Sample Sensitivity

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Solution Overview

Problem

Current methods for measuring biological materials in liquid samples, such as bacteria, are either complex, require extensive training, or struggle with sensitivity and data interpretation, particularly in determining concentration and growth rates.

Innovation Solution

A system utilizing an integrating sphere with a sample holder that allows light to be diffused and collected multiple times, enhancing sensitivity, combined with a modulated light source and phase-sensitive detection to measure scattered light, enabling precise monitoring of biological materials.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If scattering spectrophotometers use intense light sources and monochromators to measure scattered light, then measurement sensitivity is improved, but device complexity increases

Engineering Contradiction:
Improvemeasurement sensitivityVSAvoiddevice complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent combines the light source, sample chamber, and integrating sphere into a single integrated unit. The integrating sphere itself serves as both the sample holder and the light collection chamber, eliminating the need for separate monochromators and complex optical paths while maintaining measurement sensitivity through multiple internal reflections.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent employs an integrating sphere with a curved internal surface that reflects light multiple times. This spherical geometry ensures uniform light distribution and maximizes the path length of light through the sample without requiring complex optical components, thereby improving sensitivity while simplifying the overall device structure.

Inventive Principle:
Principle #14Spheroidality (Curvature)

2Measurement precision

If flow cytometers use sheath-flow and narrow tubes to force individual cell passage, then cell counting accuracy is improved, but operational complexity and training requirements increase

Engineering Contradiction:
Improvecell counting accuracyVSAvoidoperational complexity
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The patent segments the sample into individual cells through dilution in liquid medium, allowing them to pass through the measurement chamber one at a time. This simplifies the measurement process by eliminating the need for complex sheath-flow mechanisms while maintaining the ability to count and analyze individual cells accurately.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system allows samples to be simply added to the integrating sphere chamber without requiring complex preparation or sheath-flow setup. The dilution process and individual cell passage occur naturally in the liquid medium, reducing operational complexity and training requirements while maintaining measurement accuracy.

Inventive Principle:
Principle #25Self-service

3Measurement precision

If nephelometers use integrating spheres to collect scattered light, then measurement sensitivity is improved, but unscattered light passes through without being collected, reducing measurement completeness

Engineering Contradiction:
Improvemeasurement sensitivityVSAvoidmeasurement completeness
Core Design Contradiction:
Measurement precisionVSLoss of information

Solution Approach 1:

The patent positions the detector at a specific angle relative to the incident light path within the integrating sphere, typically at 90 degrees. This angular arrangement allows the detector to capture scattered light that has been redirected by particles, while the integrating sphere's internal reflections ensure that both scattered and unscattered light contribute to the overall measurement signal, providing a more complete characterization of the sample.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for highly sensitive and accurate measurement of biological samples, including pathogen growth, with faster detection times and reduced operational complexity, achieving significant improvements over existing technologies.

Implementation Method 1

Light inside the cavity is reflected multiple times off the internal surface to produce a uniform distribution of light throughout the interior of the cavity

Methodology Applied
Scientific EffectMultiple reflection: Reflection

Implementation Method 2

The hollow spherical cavity of the integrating sphere acts as a light diffusion and collection chamber

Methodology Applied
Scientific EffectDiffusion: Diffusion

Implementation Method 3

Light is incident on a sample and may be scattered by particles in the sample before entering the integrating sphere

Methodology Applied
Scientific EffectScattering: Scattering

Implementation Method 4

combined with a modulated light source and phase-sensitive detection to measure scattered light

Methodology Applied
Scientific EffectPhase-sensitive detection:

Data Source

PatentEP3256840B1Systems and methods using an integrated sphere light collector
Publication Date: 2023.08.09 UNIV COURT OF THE UNIV OF ST ANDREWS
  • EP3256840B1 patent drawingFigure 1~2
  • EP3256840B1 patent drawingFigure 3(a)~3(b)(ii)
  • EP3256840B1 patent drawingFigure 4(a)~4(c)

AI summary

A system for measuring a sample comprising: an integrating sphere light collector (12) for collecting light and containing the sample; a light source (24) for introducing light in the integrating sphere light collector (12), wherein the light source (24) is operable to output light with a known modulation, preferably by using a signal generator (26); a detector (22) for detecting scattered light in the integrating sphere light collector (12) and generating a signal indicative of the scattered light, and a lock-in amplifier (28) operable use the known light modulation and the signal generated by the detector (22) to provide an output for analysis.