Inorganic Filtration Medium With Intermeshing Paths to Reduce Voids

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Solution Overview

Problem

Existing methods for manufacturing porous monolithic inorganic supports for filtration membranes require multiple sintering operations, involve organic binders that burn during sintering, and result in voids that reduce mechanical resistance and channel quality, especially in non-rectilinear channels.

Innovation Solution

A 3D printing method using a movable extrusion head to deposit material in a controlled manner, creating rounded perimeter reliefs and avoiding voids by overlapping and crossing paths, ensuring a porous structure with controlled dimensions and turbulence-inducing channels.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If conventional extrusion and sintering methods are used to manufacture porous supports, then the support can be produced with required strength and porous texture, but multiple sintering operations are required and organic binders burn completely during sintering, complicating the process

Engineering Contradiction:
Improvemechanical resistanceVSAvoidnumber of sintering operations
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent removes organic binders from the inorganic composition entirely, replacing them with inorganic filler materials. This extraction of the harmful organic component eliminates the need for binder combustion during sintering, thereby reducing the number of sintering operations required while maintaining mechanical strength through the inorganic filler framework

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the chemical composition parameters by formulating an inorganic composition containing inorganic binder and inorganic filler materials instead of organic binders. This parameter change in material composition allows the support to achieve required mechanical strength through sintering without the complexity of organic binder combustion cycles

Inventive Principle:
Principle #35Parameter changes

2Strength

If powder bed deposition technique is used to prepare filtration membranes, then mechanically resistant supports suitable for tangential filtration can be obtained, but the fluidity of powder must be adjusted and unconsolidated powder removal is tricky, long and expensive

Engineering Contradiction:
Improvemechanical resistanceVSAvoidunconsolidated powder removal time
Core Design Contradiction:
StrengthVSLoss of time

Solution Approach 1:

The patent extracts and eliminates the unconsolidated powder removal step by using an extrusion-based additive manufacturing approach. Instead of depositing powder beds that require subsequent removal of unconsolidated material, the invention directly extrudes consolidated inorganic material layer by layer, building the support structure without generating removable unconsolidated powder

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent replaces the powder bed deposition mechanical system with an extrusion-based material deposition system. The extrusion head directly deposits and consolidates inorganic material in the desired shape, substituting the multi-step powder bed process with a continuous extrusion process that eliminates the time-consuming powder removal step

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Adaptability or versatility

If cords of material are deposited in vertical stacks to form layers, then the structure can be built from digital 3D model, but voids of material greater than pore size are created that reduce mechanical resistance

Engineering Contradiction:
Improveshape variabilityVSAvoidmechanical resistance
Core Design Contradiction:
Adaptability or versatilityVSStrength

Solution Approach 1:

The patent applies preliminary action by using computational algorithms to pre-calculate and optimize the extrusion path before manufacturing. The path planning algorithm determines the precise trajectory and deposition pattern that ensures complete wall filling without voids, while maintaining the adaptability to create complex non-rectilinear channel shapes from digital 3D models

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent introduces an intermediary computational path planning system that mediates between the digital 3D model and the physical extrusion process. This intermediary algorithm generates optimized deposition paths that ensure complete material coverage and eliminate voids, bridging the gap between design flexibility and structural integrity

Inventive Principle:
Principle #24Intermediary (Mediator)

4Strength

If staggered pattern deposition is used to avoid voids, then some empty spaces are reduced, but the quality of lateral surfaces deteriorates and gaps lead to collapse of upper layer material deposit

Engineering Contradiction:
Improvemechanical resistanceVSAvoidlateral surface quality
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent uses preliminary computational path optimization to determine the precise extrusion trajectory that maintains lateral surface quality. The algorithm calculates optimal deposition patterns that ensure each layer is properly supported by the previous layer, preventing collapse while avoiding void formation, thus maintaining both structural integrity and surface quality

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces a mechanically resistant, porous support with controlled porosity and channel dimensions, reducing pressure losses and enhancing filtration efficiency.

Implementation Method 1

An inorganic composition emerges from the extrusion head in the form of a ribbon of material or cord making it possible to build, from a digital 3D model, a raw, manipulable three-dimensional structure

Methodology Applied
Scientific EffectExtrusion: Extrusion

Implementation Method 2

The porous support is prepared by a technique proceeding by addition of material... The raw, manipulable three-dimensional structure is then subjected to a sintering step

Methodology Applied
Scientific EffectSintering: Sintering

Implementation Method 3

rounded perimeter reliefs on the wall of at least one circulation channel, participating in the generation of turbulence

Methodology Applied
Scientific EffectTurbulence: Turbulence

Data Source

PatentEP4457065B1Method for producing an inorganic filtration medium through intermeshing and obtained membrane
Publication Date: 2025.09.17 TECHNOLOGIES AVANCEES ET MEMBRANES INDUSTRIELLES SA
  • EP4457065B1 patent drawingFigure 1A~1C
  • EP4457065B1 patent drawingFigure 1D~2A
  • EP4457065B1 patent drawingFigure 2B

AI summary

The invention relates to a method for producing a porous monolithic inorganic medium (1) using a 3D printing machine comprising at least one extruder head (6) mounted so as to be moveable in space, the method consisting in: - driving the extruder head along a numerical trajectory so that: * for a path with overlap, the material being deposited partially overlaps at least one edge of a previously deposited deposit of material by a portion of overlapping material within its thickness and whose thickness is strictly less than the nominal height (e) so as to avoid gaps between the rounded edges of the deposit of material currently being deposited and those of the previously deposited deposit of material; * for a path with intersection, the material currently being deposited intersects with at least one previously deposited deposit of material that completely overlaps with the previously deposited deposit of material by a portion of overlapping material within its thickness and whose thickness is strictly less than the nominal height (e).