Ion Analyzer Additive Flow Control for Contamination Reduction

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Solution Overview

Problem

Existing additive mixing methods in ion analyzers lead to contamination of the apparatus, increased power consumption, and slow switching between additives, resulting in reduced sensitivity and robustness, as well as inefficient reaction timing with measurement target substances.

Innovation Solution

An ion analyzer design that includes a spray unit for atomizing and spraying a liquid additive only when necessary, with a control unit to adjust the flow rate of the additive, preventing contamination and allowing quick switching between additives by separating the sample and additive flow passages and optimizing their interaction with the measurement target substance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If the additive is continuously supplied to the spray unit, then the measurement target substance can be consistently ionized with high sensitivity, but the apparatus becomes contaminated with the additive, reducing robustness and requiring frequent maintenance

Engineering Contradiction:
ImprovesensitivityVSAvoidrobustness
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The control unit controls the supply of additive to the spray unit in a periodic manner, supplying the additive only during periods when measurement target substance is being introduced. This periodic supply maintains high sensitivity during measurement while preventing continuous contamination that would reduce robustness and require frequent maintenance.

Inventive Principle:
Principle #19Periodic action

2Productivity

If the flow rate of additive is increased to ensure sufficient reaction with measurement target substance, then ionization efficiency improves, but the contamination of apparatus increases and switching between additives becomes slower

Engineering Contradiction:
Improveionization efficiencyVSAvoidswitching time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The flow rate of additive is dynamically adjusted by the control unit based on the presence and concentration of measurement target substance. When measurement target substance is detected, the additive flow rate is increased to ensure sufficient reaction and high ionization efficiency. When no target substance is present, the flow rate is reduced or stopped, enabling faster switching between additives and reducing contamination.

Inventive Principle:
Principle #15Dynamics

3Ease of operation

If the additive flow passage is heated to prevent condensation and contamination, then the additive can be supplied smoothly, but the power consumption increases

Engineering Contradiction:
Improveadditive supply stabilityVSAvoidpower consumption
Core Design Contradiction:
Ease of operationVSUse of energy by moving object

Solution Approach 1:

The heating of the additive flow passage is controlled periodically, being activated only during periods when additive is being supplied. This periodic heating prevents condensation and ensures smooth additive supply during operation, while avoiding continuous power consumption when additive supply is not required.

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design minimizes contamination, reduces power consumption, and enables rapid switching between additives, maintaining high sensitivity and robustness while ensuring efficient reactions with measurement target substances.

Implementation Method 1

a spray unit for atomizing and spraying toward the measurement target substance a liquid containing an additive

Methodology Applied
Scientific EffectAtomization:

Implementation Method 2

an ion source for ionizing a measurement target substance

Methodology Applied
Scientific EffectIonization: Ionisation

Implementation Method 3

a separation analysis unit for separately analyzing an ion generated by a reaction between the measurement target substance and the additive

Methodology Applied
Scientific EffectMagnetic field separation: Magnetic Field

Implementation Method 4

a separation analysis unit for separately analyzing an ion generated by a reaction between the measurement target substance and the additive

Methodology Applied
Scientific EffectElectric field separation: Electric Field

Implementation Method 5

a detector for detecting the ion that has been separately analyzed by the separation analysis unit

Methodology Applied
Scientific EffectIon detection:

Data Source

PatentUS10431445B2Ion analysis device
Publication Date: 2019.10.01 HITACHI HIGH TECH CORP
  • US10431445B2 patent drawing
  • US10431445B2 patent drawing
  • US10431445B2 patent drawing

AI summary

To reduce contamination of the apparatus with an additive and to quickly switch spraying and stopping of the additive, provided is an ion analyzer including: an ion source for ionizing a measurement target substance, a spray unit for atomizing and spraying toward the measurement target substance a liquid containing an additive that reacts with the measurement target substance; a separation analysis unit for separately analyzing an ion generated by a reaction between the measurement target substance and the additive; a detector for detecting the ion that has been separately analyzed by the separation analysis unit; and a control unit for lowering a flow rate of the additive supplied to the spray unit during a time when the additive is not necessary.