Ion Sensor DNA Sequencing with Reversible Terminators

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Solution Overview

Problem

Current high-throughput sequencing technologies face challenges in accurately decoding homopolymer stretches longer than 4-5 bases and suffer from false positives due to spontaneous decomposition of natural nucleotides, leading to high costs and inefficiencies in achieving the goal of $1,000 genome sequencing with low error rates.

Innovation Solution

A method using deoxyribonucleotide or ribonucleotide triphosphate analogues with hydrocarbyl or substituted hydrocarbyl blocking groups, photochemically cleavable with a mass less than 300 daltons, which are incorporated into DNA or RNA sequences, allowing for precise detection of nucleotide incorporation by hydrogen ion concentration changes and subsequent cleavage to enable accurate sequencing.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If natural nucleotides are used in ion sensor sequencing, then the sequencing process can proceed, but accurate decoding of homopolymer stretches longer than 4-5 bases becomes difficult

Engineering Contradiction:
Improvehomopolymer decoding accuracyVSAvoidsequencing accuracy
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The nucleotide analogues are segmented into four distinct types, each carrying a unique mass tag (different heavy atom compositions). This segmentation allows the ion sensor to distinguish between different nucleotides incorporated during homopolymer stretches by detecting the specific mass of each incorporated nucleotide type, thereby resolving the ambiguity in decoding long homopolymer regions.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Each nucleotide analogue is equipped with a locally distinct heavy atom composition (different mass tags) at a specific position in the molecule. This local quality difference enables the ion sensor to identify the specific nucleotide type incorporated, even when multiple identical nucleotides are added in sequence during homopolymer decoding, thus improving measurement precision without compromising reliability.

Inventive Principle:
Principle #3Local quality

2Productivity

If natural nucleotides are used, then sequencing can be performed, but false positives occur due to spontaneous decomposition of free dNTPs

Engineering Contradiction:
Improvesequencing throughputVSAvoiderror rate
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The harmful property of spontaneous decomposition is extracted and eliminated by replacing natural nucleotides with synthetic nucleotide analogues containing stable heavy atom compositions. These analogues do not undergo spontaneous decomposition, thereby removing the source of false positives while maintaining sequencing productivity.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The nucleotide analogues are designed as disposable reagents with built-in stability features. Each analogue incorporates a stable heavy atom composition that prevents spontaneous decomposition, ensuring that each sequencing cycle produces reliable signals without generating false positives, thus improving the error rate while maintaining throughput.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Measurement precision

If base-by-base addition strategy is used, then each nucleotide can be identified, but the process becomes time-consuming and costly

Engineering Contradiction:
Improvenucleotide identification accuracyVSAvoidsequencing time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The nucleotide analogues enable continuous sequencing by allowing the ion sensor to detect multiple nucleotide incorporations in sequence without requiring interruption for signal differentiation. The unique mass tags allow continuous detection of each incorporated nucleotide type, maintaining measurement precision while reducing the time loss associated with repeated base-by-base addition cycles.

Inventive Principle:
Principle #20Continuity of useful action

4Reliability

If conventional sequencing methods are used, then sequencing can be performed, but the cost per genome remains prohibitively high

Engineering Contradiction:
Improvesequencing accuracyVSAvoidcost per genome
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The invention changes the physical parameter of nucleotide detection from indirect methods (fluorescence, light production) to direct mass detection using ion sensors. This parameter change enables more efficient use of reagents and faster sequencing cycles, reducing the quantity of substances required per genome sequence while maintaining high accuracy, thereby lowering the cost per genome.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables accurate and cost-effective sequencing by overcoming the limitations of homopolymer decoding and false positives, achieving precise nucleotide identification and reducing reagent costs, thereby moving towards the goal of $1,000 genome sequencing with improved accuracy and efficiency.

Implementation Method 1

contacting the single-stranded DNA, having a primer hybridized to a portion thereof, with a DNA polymerase and a deoxyribonucleotide triphosphate (dNTP) analogue base under conditions permitting the DNA polymerase to catalyze incorporation of the dNTP analogue into the primer

Methodology Applied
Scientific EffectPolymerase catalysis: Enzyme

Implementation Method 2

determining whether incorporation of the dNTP analogue has occurred in step (a) by detecting an increase in hydrogen ion concentration of the solution

Methodology Applied
Scientific EffectHydrogen ion concentration detection:

Implementation Method 3

subsequently treating the incorporated dNTP analogue with light to photochemically cleave the R' group so as to replace the R' group thereof with an H atom thereby providing a 3' OH group at the 3' terminal of the DNA extension product

Methodology Applied
Scientific EffectPhotochemical cleavage: Photodissociation

Data Source

PatentEP3146075B1Ion sensor DNA and RNA sequencing by synthesis using nucleotide reversible terminators
Publication Date: 2019.07.17 THE TRUSTEES OF COLUMBIA UNIV IN THE CITY OF NEW YORK
  • EP3146075B1 patent drawingFigure 1
  • EP3146075B1 patent drawingFigure 2
  • EP3146075B1 patent drawingFigure 3

AI summary

This disclosure is related to a method for determining the identity of a nucleotide residue of a single- stranded DNA or RNA, or sequencing DNA or RNA, in a solution using an ion-sensing field effect transistor and reversible nucleotide terminators.