Etched Ion-Track Battery Separator for Polysulfide Shuttle Suppression

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Solution Overview

Problem

Lithium-sulfur batteries and other cationic ion batteries face challenges due to the polysulfide redox shuttle phenomenon, leading to self-discharge and performance deterioration, with existing solutions being either costly or limited in effectiveness.

Innovation Solution

A porous polymer etched ion-track membrane is used as a separator, featuring nanochannels with controlled dimensions and geometry, which allows cationic ion flux while suppressing polysulfides, enhancing coulombic efficiency and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a conventional porous separator is used, then ion transport is enabled, but polysulfide shuttle phenomenon occurs leading to self-discharge and performance deterioration

Engineering Contradiction:
Improvebattery stabilityVSAvoidpolysulfide shuttle
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent employs a porous polymer etched ion-track membrane with precisely controlled nanochannels (10-200 nm diameter) as the separator. The porous structure enables cationic ion transport while the specific nanoscale pore dimensions physically block polysulfide molecules, resolving the contradiction between enabling ion flow and preventing polysulfide shuttle phenomenon

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The separator features asymmetric nanochannel geometry with different opening diameters at each surface, creating local quality variations. The narrower openings at one surface provide enhanced polysulfide blocking while maintaining adequate ion transport pathways, allowing the separator to simultaneously achieve selective transport and structural stability

Inventive Principle:
Principle #3Local quality

2Reliability

If existing solutions to suppress polysulfide shuttle are implemented, then battery performance is improved, but manufacturing cost increases or effectiveness is limited

Engineering Contradiction:
Improvecoulombic efficiencyVSAvoidmanufacturing cost
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent achieves superior polysulfide blocking by precisely controlling the nanochannel diameter parameter (10-200 nm range) through ion-track etching process variables such as ion fluence, etching time, and chemical composition. This parameter optimization enables effective polysulfide suppression using conventional polymer materials, avoiding the need for expensive alternative solutions while maintaining high coulombic efficiency

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses commercially available polymer films (polyethylene terephthalate, polycarbonate, polyethylene, polypropylene, polyimide, polytetrafluoroethylene, or polyvinylidene fluoride) as the base material for the separator. These inexpensive, readily available materials are transformed into high-performance separators through the ion-track etching process, providing a cost-effective solution compared to specialized expensive materials

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Object-generated harmful factors

If the separator pores are made smaller to block polysulfides, then polysulfide shuttle is reduced, but ion flux may be restricted

Engineering Contradiction:
Improvepolysulfide blockingVSAvoidion transport rate
Core Design Contradiction:
Object-generated harmful factorsVSSpeed

Solution Approach 1:

The patent applies partial action by creating nanochannels with diameters (10-200 nm) that are sufficiently small to block polysulfide molecules yet large enough to maintain adequate ion transport. The asymmetric pore geometry with different opening diameters at each surface optimizes this balance, providing enhanced polysulfide rejection at the critical interface while preserving ion flux through the membrane bulk

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The membrane effectively reduces the polysulfide shuttle, improving the cycling stability and coulombic efficiency of lithium-sulfur batteries and other cationic ion batteries, offering a cost-effective and scalable solution.

Implementation Method 1

the membrane comprises a plurality of nanochannels, the majority in number of said nanochannels is continuous and has an opening tip at the frontside and an opening tip at the backside of said membrane

Methodology Applied
Scientific EffectIon transport through porous membrane: Permeation

Implementation Method 2

which allows cationic ion flux while suppressing polysulfides

Methodology Applied
Scientific EffectPhysical blocking of polysulfides: Filter (physical)

Implementation Method 3

an appropriate porous structure, in order to make possible the diffusion of the anions and cations of the electrolyte

Methodology Applied
Scientific EffectDiffusion of cations: Diffusion

Data Source

PatentEP3639310B1Use of a porous polymer etched ion-track membrane as a separator for a battery
Publication Date: 2023.09.13 GSI HELMHOLTZZENT FUR SCHWERIONENFORSCHUNG GMBH
  • EP3639310B1 patent drawingFigure 1~2
  • EP3639310B1 patent drawingFigure 3~4
  • EP3639310B1 patent drawingFigure 5~5(b)

AI summary

The present invention relates to the use of a porous polymer etched ion-track membrane as separator for batteries comprising a positive electrode, a negative electrode and a liquid electrolyte comprising at least one salt of a cationic ion in solution in a solvent, and to batteries comprising such a membrane as porous separator.