Ionic Liquid Fiber Welding for Scalable Natural Fiber Composites

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Traditional methods for producing natural fiber composites are limited by the physical constraints of dissolving biopolymers, leading to disrupted structures and reduced control over the final product properties, particularly in scaling up processes beyond benchtop levels.

Innovation Solution

The fiber welding process uses ionic liquid-based solvents to partially dissolve natural fibers, allowing for the manipulation and fusion of fibers into desired shapes without fully denaturing the biopolymers, enabling the production of robust composite materials with retained original material properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If biopolymers are fully dissolved in solution to create composite materials, then the material can be easily processed and formed into desired shapes, but the original fiber structure is disrupted and material properties are reduced

Engineering Contradiction:
ImproveprocessabilityVSAvoidmaterial properties
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The patent applies partial dissolution by using ionic liquid solvents that selectively dissolve the matrix material surrounding the fibers while leaving the fiber cores intact. This partial action allows the matrix to be processed and reformed while preserving the structural integrity and material properties of the embedded fibers, resolving the contradiction between ease of manufacture and strength.

Inventive Principle:
Principle #16Partial or excessive action

2Strength

If traditional solvent-based welding is used to fuse natural fibers, then fiber bonding is achieved, but the process is limited to benchtop scale and cannot be easily scaled up

Engineering Contradiction:
Improvefiber bondingVSAvoidscalability
Core Design Contradiction:
StrengthVSProductivity

Solution Approach 1:

The patent changes the chemical parameters of the welding process by employing ionic liquid solvents with specific properties (high thermal stability, tunable solubility) that enable the process to be conducted at elevated temperatures and extended durations. These parameter changes allow transition from benchtop to industrial scale while maintaining effective fiber bonding through controlled partial dissolution and reformation.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If high concentrations of biopolymer are dissolved in solution (e.g., 10% cotton with 90% ionic liquid), then more material can be processed, but the solution becomes viscous and difficult to handle

Engineering Contradiction:
Improvebiopolymer concentrationVSAvoidhandling difficulty
Core Design Contradiction:
Quantity of substanceVSEase of operation

Solution Approach 1:

The patent applies preliminary action by pre-forming the fiber architecture and structure before introducing the ionic liquid solvent. The fibers are arranged in the desired configuration and partially dissolved in advance, allowing the viscous high-concentration solution to be applied to pre-formed structures rather than attempting to handle and form the viscous material from scratch, thereby improving ease of operation despite high biopolymer concentration.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for the creation of composite materials with enhanced physical and chemical properties, such as increased tensile strength and hydrophobicity, while reducing the need for glues or resins, and enables scalable production of high-quality materials from natural fibers.

Implementation Method 1

Ionic liquids (e.g., 1-ethyl-3-methylimidazolium acetate) can dissolve natural fiber biopolymers (e.g., cellulose and silk) without derivatization. Natural fiber welding is a process by which biopolymer fibers are fused in a manner roughly analogous to traditional plastic welding.

Methodology Applied
Scientific EffectPartial dissolution: Solvation

Implementation Method 2

Natural fiber welding is a process by which biopolymer fibers are fused in a manner roughly analogous to traditional plastic welding.

Methodology Applied
Scientific EffectFusion welding: Welding

Data Source

PatentUS11555263B2Methods, processes, and apparatuses for producing dyed and welded substrates
Publication Date: 2023.01.17 NATURAL FIBER WELDING INC
  • US11555263B2 patent drawing
  • US11555263B2 patent drawing
  • US11555263B2 patent drawing

AI summary

A dyeing and welding process may be configured to convert a substrate into a welded substrate having at least some color imparted thereto via a dye and/or coloring agent by applying a process solvent having a dye and/or coloring agent therein to the substrate, wherein the process solvent interrupts one or more intermolecular force between one or more component in the substrate. The substrate may be configured as a natural fiber, such as cellulose, hemicelluloses, and silk. The process solvent may include a binder, such as dissolved biopolymer (e.g., cellulose). After application of a process solvent comprised of a dye and/or coloring agent, the substrate may be exposed to a second application of a process solvent comprised of a binder, which second application may occur before or after a process temperature/pressure zone, process solvent recovery zone, and/or drying zone.