Ionic Liquid Peroxide Decomposition for Low-Temperature Oxygen Generation

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Solution Overview

Problem

Existing oxygen generation methods, such as chlorate candles and peroxide-based systems, face challenges including high temperature requirements, production of toxic byproducts, system instability, and inefficiency at subfreezing temperatures, which limit their reliability and safety in emergency oxygen supply systems.

Innovation Solution

The use of ionic liquids with metallate anions to decompose solid peroxide compounds at low temperatures, providing a method for continuous oxygen production without toxic byproducts, using a composition that includes a peroxide compound and an ionic liquid as a solvent and heat sink, allowing for extended oxygen generation with a significant flow rate.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If chlorate candles are used for oxygen generation, then oxygen can be produced, but high temperatures (450-700°C) are required which necessitate heat insulation and increase weight and size

Engineering Contradiction:
Improveoxygen productionVSAvoidweight of oxygen generator
Core Design Contradiction:
Quantity of substanceVSWeight of moving object

Solution Approach 1:

The invention changes the temperature parameter from high (450-700°C in chlorate candles) to low (below 150°C, preferably below 100°C) by using peroxide compounds as oxygen source instead of chlorates, eliminating the need for heat insulation and reducing weight

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention extracts and removes the heat insulation component entirely by eliminating the high-temperature reaction requirement, taking out the problematic thermal management system that added weight and complexity

Inventive Principle:
Principle #2Taking out (Extraction)

2Quantity of substance

If chlorate candles are used for oxygen generation, then oxygen can be produced, but toxic side products (chlorine) are generated which must be removed, adding size and weight

Engineering Contradiction:
Improveoxygen productionVSAvoidtoxic byproducts
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The invention converts the harmful chlorate decomposition reaction into a beneficial peroxide decomposition reaction that produces only oxygen and water, eliminating toxic chlorine byproducts while maintaining oxygen generation capability

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The invention extracts and eliminates the toxic chlorine byproduct formation by replacing chlorate chemistry with peroxide chemistry, removing the need for toxic gas removal systems

Inventive Principle:
Principle #2Taking out (Extraction)

3Quantity of substance

If peroxide-based oxygen generators use water for catalyst contact, then oxygen can be produced, but the system fails below 0°C because water freezes

Engineering Contradiction:
Improveoxygen productionVSAvoidtemperature range
Core Design Contradiction:
Quantity of substanceVSAdaptability or versatility

Solution Approach 1:

The invention changes the solvent parameter from water (freezing point 0°C) to organic solvent (remaining liquid below 0°C), enabling oxygen generation in subfreezing temperatures while maintaining catalyst solubility and reaction functionality

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention applies local quality by using different solvent properties in different temperature regimes, selecting organic solvents specifically for their low-temperature liquid state to enable operation in cold environments

Inventive Principle:
Principle #3Local quality

4Quantity of substance

If peroxide-based oxygen generators use aqueous solutions, then oxygen can be produced, but vehement effervescing occurs requiring complicated device structure

Engineering Contradiction:
Improveoxygen productionVSAvoiddevice structure
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The invention changes the reaction medium parameter from aqueous solution to organic solvent, which suppresses effervescing and foaming during oxygen evolution, allowing for simpler device structure without complex foam control mechanisms

Inventive Principle:
Principle #35Parameter changes

5Quantity of substance

If chlorate candles use liquid zone for reaction, then decomposition can proceed, but mechanical shocks or vibrations may separate candle portions, interrupting heat transfer and oxygen production

Engineering Contradiction:
Improveoxygen productionVSAvoidsystem stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The invention changes the physical state parameter of the reaction medium from liquid (unstable, separates under shock) to solid (stable, maintains structural integrity), using solid peroxide compounds that remain intact under mechanical stress while still enabling decomposition reaction

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables reliable and continuous oxygen production at low temperatures, below 150°C, without toxic components, and over an extended period, improving the safety and efficiency of emergency oxygen supply systems.

Implementation Method 1

using a composition that includes a peroxide compound and an ionic liquid as a solvent and heat sink

Methodology Applied
Scientific EffectHeat sink: Heat Sink

Implementation Method 2

The use of ionic liquids with metallate anions to decompose solid peroxide compounds at low temperatures

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP3323779B1Method for generating oxygen using ionic liquids for decomposing peroxides
Publication Date: 2020.06.03 DIEHL AVIATION GILCHING GMBH
  • EP3323779B1 patent drawingFigure 1
  • EP3323779B1 patent drawingFigure 2
  • EP3323779B1 patent drawingFigure 3

AI summary

The present invention relates to a method for generating oxygen, comprising providing at least one oxygen source, providing at least one ionic liquid, the ionic liquid comprising a cation and an anion, wherein the oxygen source is a hydrogen peroxide adduct compound which is at least partially soluble in the ionic liquid, the ionic liquid is in the liquid state at least in a temperature range from -10°C to +50°C, and the anion is selected from metallate anions, and contacting the oxygen source and the ionic liquid.