Ionic Liquid Purification Composition Viscosity Control

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Solution Overview

Problem

Existing organic material purification methods face challenges in efficiently purifying organic materials for organic light emitting devices, particularly due to high viscosity of ionic liquids at ambient temperatures, which hinders solubility and processing efficiency, and often require additional processing steps or high temperatures.

Innovation Solution

A mixed composition of an ionic liquid and an organic solvent, such as alcohol or ketone, is used to create a purification solution with a viscosity of 15 cP or less at 20° C. to 25° C., allowing for effective separation and purification of organic materials with different polarities at ambient temperature without the need for high pressure filters or significant changes in temperature or pressure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If ionic liquid is used for purification, then purification effectiveness is improved, but viscosity increases making processing difficult

Engineering Contradiction:
Improvepurification effectivenessVSAvoidprocessing ease
Core Design Contradiction:
Manufacturing precisionVSEase of operation

Solution Approach 1:

The patent combines ionic liquid with organic solvent to create a composite purification composition. The ionic liquid provides purification effectiveness through selective solubility, while the organic solvent reduces viscosity to improve processability. This composite approach allows both benefits to coexist without compromising either purification quality or handling ease.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent modifies the physical parameters of the purification medium by adjusting the ratio of ionic liquid to organic solvent, controlling viscosity within a specific range (10-50 cP). This parameter optimization ensures the composition remains fluid enough for easy processing while maintaining sufficient ionic liquid content for effective purification.

Inventive Principle:
Principle #35Parameter changes

2Stability of the object's composition

If high temperature is used for purification, then solubility is improved, but energy consumption and equipment requirements increase

Engineering Contradiction:
ImprovesolubilityVSAvoidenergy consumption
Core Design Contradiction:
Stability of the object's compositionVSUse of energy by moving object

Solution Approach 1:

The patent changes the chemical composition parameters of the purification medium by introducing organic solvent, which modifies the solubility characteristics of the system. This allows effective purification to occur at ambient temperature rather than requiring elevated temperatures, thereby reducing energy consumption and equipment complexity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The organic solvent acts as an intermediary substance that facilitates the dissolution and separation processes at lower temperatures. It mediates between the ionic liquid and the organic material to be purified, enabling effective purification without the need for high temperature conditions.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If additional processing steps are added, then purification quality is improved, but process complexity increases

Engineering Contradiction:
Improvepurification qualityVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent merges the functions of multiple processing steps into a single purification composition. The combined ionic liquid-organic solvent system performs both dissolution and selective separation in one step, eliminating the need for multiple sequential processing steps while maintaining high purification quality.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The purification composition exhibits multi-functionality by simultaneously providing solubility enhancement, selective separation, and viscosity control within a single system. This universal composition replaces multiple specialized processing steps, simplifying the overall process while maintaining or improving purification quality.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables efficient purification of organic materials at ambient temperature, reducing processing time and cost, while maintaining high purity and allowing for the recycling of the ionic liquid, thus addressing the limitations of existing methods.

Implementation Method 1

A mixed composition of an ionic liquid and an organic solvent, such as alcohol or ketone, is used to create a purification solution with a viscosity of 15 cP or less at 20° C. to 25° C.

Methodology Applied
Scientific EffectSolvation: Solvation

Implementation Method 2

allowing for effective separation and purification of organic materials with different polarities at ambient temperature

Methodology Applied
Scientific EffectDifferential solubility: Solvation

Data Source

PatentUS10919007B2Organic material purification composition and method of purifying organic materials using the same
Publication Date: 2021.02.16 SAMSUNG DISPLAY CO LTD
  • US10919007B2 patent drawing
  • US10919007B2 patent drawing
  • US10919007B2 patent drawing

AI summary

An organic material purification composition, a mixed composition, and a method of purifying an organic material, the organic material purification composition including an ionic liquid in which a cation and an anion are combined; and an organic solvent, wherein the organic solvent includes an alcohol or a ketone.