Infrared-absorbing Coated Backing Plate for MBE Temperature Control

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Solution Overview

Problem

Molecular beam epitaxy (MBE) deposition processes face temperature instability due to high absorption in the growth film, particularly when growing low bandgap materials on high bandgap substrates, leading to uncontrolled surface temperature increases and compromised film quality.

Innovation Solution

A thermally conductive backing plate with an infrared-absorbing coating (IAC) is used to absorb radiant heat from the heater and conductively transfer it to the substrate, decoupling radiative heating and maintaining precise temperature control during film growth, allowing for efficient heating of the substrate to elevated temperatures without direct contact.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If radiative heating is used to heat the substrate during MBE deposition, then heating efficiency is improved, but temperature control stability deteriorates due to uncontrolled temperature increases from high absorption in the growth film

Engineering Contradiction:
Improveheating efficiencyVSAvoidtemperature control stability
Core Design Contradiction:
Use of energy by moving objectVSStability of the object's composition

Solution Approach 1:

A thermally conductive backing plate with an infrared-absorbing coating is introduced as an intermediary between the heater and the substrate. The coating absorbs infrared radiation from the heater and converts it to heat, which is then conductively transferred to the substrate. This mediator enables efficient radiative heating while the thick backing plate provides thermal mass and conductive coupling to stabilize temperature, preventing uncontrolled temperature increases.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The heating system uses a composite structure combining an infrared-absorbing coating (such as amorphous silicon, amorphous germanium, or their alloys) with a thermally conductive backing plate (such as molybdenum, tungsten, or their alloys). The coating layer has high infrared absorption coefficient while the backing plate has high thermal conductivity, creating a composite system that achieves both efficient heating and stable temperature control.

Inventive Principle:
Principle #40Composite materials

2Speed

If direct radiative coupling between heater and substrate is used, then heating speed is improved, but film quality deteriorates due to temperature instability during deposition

Engineering Contradiction:
Improveheating speedVSAvoidfilm quality
Core Design Contradiction:
SpeedVSManufacturing precision

Solution Approach 1:

The infrared-absorbing coating on the backing plate serves as a mediator that intercepts infrared radiation from the heater and converts it to conductive heat transfer. This allows rapid heating through radiative absorption while the thick thermally conductive backing plate acts as a heat reservoir that stabilizes temperature fluctuations, ensuring consistent film quality during deposition.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The system changes the heat transfer mechanism from direct radiative coupling to a two-stage process: radiative absorption by the coating followed by conductive transfer through the backing plate. This parameter change in heat transfer mode enables both fast heating (through radiative absorption) and temperature stability (through conductive coupling and thermal mass), thereby maintaining high film quality.

Inventive Principle:
Principle #35Parameter changes

3Measurement precision

If infrared-absorbing coating is applied to the backing plate, then temperature control precision is improved, but device complexity increases

Engineering Contradiction:
Improvetemperature control precisionVSAvoiddevice complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The solution uses a composite structure of a thin infrared-absorbing coating (e.g., amorphous silicon or germanium layer) deposited on a conventional thermally conductive backing plate. This composite approach achieves precise temperature control through the coating's selective infrared absorption while relying on the well-understood thermal properties of the backing plate material, avoiding the need for complex active control systems.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention changes the optical parameter of the backing plate by adding an infrared-absorbing coating, transforming it from a purely thermally conductive component to a radiatively active thermal management component. This simple parameter change (adding coating layer) achieves precise temperature control without introducing complex control mechanisms or multiple moving parts.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution enables stable temperature control and uniform heating of the substrate, preventing temperature spikes and ensuring consistent film quality by maintaining the substrate and film at a desired temperature, even for low bandgap materials like GeTe on GaAs substrates, facilitating the growth of high-quality thin films.

Implementation Method 1

at least the first surface includes an infrared-absorbing coating (IAC) thereon... the heater is positioned to emit IR through a portion of the UHV chamber and impinge the IAC

Methodology Applied
Scientific EffectInfrared radiation absorption: Absorption (EM radiation)

Implementation Method 2

a thermally conductive backing plate... thermally conducting heat from the non-coated side of the thermally conductive backing plate to a substrate

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Data Source

PatentUS11926925B2Molecular-beam epitaxy system comprising an infrared radiation emitting heater and a thermally conductive backing plate including an infrared-absorbing coating thereon
Publication Date: 2024.03.12 JOHNS HOPKINS UNIVERSITY
  • US11926925B2 patent drawing
  • US11926925B2 patent drawing
  • US11926925B2 patent drawing

AI summary

Methods and systems for growing thin films via molecular-beam epitaxy (MBE) on substrates are provided. The methods and systems utilize a thermally conductive backing plate including an infrared-absorbing coating (IAC) formed, for example, on one side of the thermally conductive backing plate to provide an asymmetric emissivity that absorbs infrared radiation (IR) on the side having the IRC and does not on the non-coated side of the thermally conductive backing plate (e.g., refractive metal or alloy). The asymmetric emissivity shields the thin film being deposited on a substrate from the IR during formation.