Irregular Silica Particles for Resin Adhesion

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Solution Overview

Problem

Silica particles used in various applications face challenges in maintaining flowability and durability due to their shape and size, as they tend to become spherical and lose adhesiveness when small, or become fragile and easily damaged when large, making it difficult to enhance the strength and flowability of attachment targets.

Innovation Solution

Silica particles with a volume average size of 100 nm to 500 nm, an average circularity degree of 0.5 to 0.85, and a ratio of circle equivalent diameters to maximum heights of 1.5 to 1.9 are developed, providing an irregular shape that maintains flowability and durability by resisting mechanical loads and attachment to surfaces.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If silica particles are made small to enhance flowability, then flowability is improved, but adhesiveness is lost

Engineering Contradiction:
ImproveflowabilityVSAvoidadhesiveness
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent applies parameter changes by precisely controlling the particle size within 100-500 nm range and circularity degree within 0.5-0.85, transforming the silica particle properties to achieve both good flowability and adhesiveness simultaneously. This resolves the contradiction by finding an optimal parameter range where both requirements are satisfied.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces the aspect ratio (Da/H ratio of 1.5-1.9) as an additional dimensional parameter to control particle morphology. By controlling not just size but also shape dimensions, the invention achieves particles that maintain flowability while enhancing adhesiveness through controlled irregularity.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Strength

If silica particles are made large to enhance strength, then strength is improved, but durability deteriorates due to increased fragility

Engineering Contradiction:
ImprovestrengthVSAvoiddurability
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent resolves this contradiction by optimizing the particle size parameter within 100-500 nm and circularity degree within 0.5-0.85, achieving a balance where particles have sufficient strength while maintaining durability through controlled morphology that resists mechanical damage.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies asymmetry by controlling the circularity degree to be 0.5-0.85, creating particles with controlled irregular shapes rather than perfect spheres. This asymmetric morphology enhances both strength and durability by distributing mechanical stresses more effectively.

Inventive Principle:
Principle #4Asymmetry

3Ease of manufacture

If silica particles become spherical to simplify shape, then manufacturing is easier, but adhesiveness is reduced

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidadhesiveness
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent resolves this contradiction by precisely controlling the circularity degree parameter within 0.5-0.85, creating particles with controlled irregularity that maintain manufacturing feasibility while significantly improving adhesiveness compared to perfectly spherical particles.

Inventive Principle:
Principle #35Parameter changes

Data Source

PatentUS8431633B2Silica particles, manufacturing method thereof and resin particles
Publication Date: 2013.04.30 FUJIFILM BUSINESS INNOVATION CORP

AI summary

Disclosed are silica particles having a volume average particle size of from about 100 nm to about 500 nm, an average circularity degree of from about 0.5 to about 0.85, and an average value of the ratios of circle equivalent diameters Da of the silica particles obtained by a flat image analysis to maximum heights H of the silica particles obtained by a stereoscopic image analysis of more than 1.5 and less than 1.9.