Isothermal CVD Reactor Wall Temperature Control

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Solution Overview

Problem

In chemical vapor deposition (CVD) processes, condensation of reaction byproducts in vacuum systems leads to equipment contamination, maintenance challenges, and yield losses due to hydroscopic byproducts absorbing moisture, causing pump failures and insulation degradation.

Innovation Solution

A double wall vacuum processing chamber with thermal insulation and a heated thermal transfer fluid system maintains the inner wall temperature above the condensation temperature of reactant and effluent gases, preventing condensation and maintaining a clean, isothermal environment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-generated harmful factors

If the chamber walls are cooled to condense byproducts, then byproduct removal is improved, but equipment contamination and maintenance challenges worsen

Engineering Contradiction:
Improvebyproduct condensationVSAvoidequipment contamination
Core Design Contradiction:
Object-generated harmful factorsVSObject-affected harmful factors

Solution Approach 1:

The patent introduces an intermediary substance (getter material) that is placed within the chamber to absorb and trap byproducts. This getter material acts as a mediator between the byproducts and the chamber walls, preventing direct condensation on equipment surfaces while still removing harmful byproducts from the atmosphere.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent extracts the byproduct removal function from the chamber walls themselves and relocates it to dedicated getter materials or traps positioned strategically within the chamber. This separation allows the walls to remain clean while byproducts are captured by the extracted removal components.

Inventive Principle:
Principle #2Taking out (Extraction)

2Object-generated harmful factors

If hydroscopic byproducts are allowed to absorb moisture, then byproduct removal is simplified, but pump reliability and process yield worsen

Engineering Contradiction:
Improvebyproduct accumulationVSAvoidpump reliability
Core Design Contradiction:
Object-generated harmful factorsVSReliability

Solution Approach 1:

The patent applies preliminary anti-action by introducing getter materials that preemptively capture hydroscopic byproducts before they can absorb moisture from the atmosphere. This preliminary capture prevents the formation of moisture-laden condensates that would otherwise damage pumps and reduce yield.

Inventive Principle:
Principle #9Preliminary anti-action

Solution Approach 2:

The patent converts the harmful hygroscopic property of certain byproducts into a beneficial trapping mechanism. By using getter materials with high affinity for these byproducts, the natural tendency of byproducts to attract and hold moisture is harnessed to concentrate and localize them in controlled trap locations rather than allowing diffuse contamination.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Productivity

If the chamber is opened for batch changes, then productivity is improved, but byproduct re-contamination and maintenance costs worsen

Engineering Contradiction:
Improvebatch change efficiencyVSAvoidatmospheric contamination
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent implements preliminary action by pre-positioning getter materials and traps throughout the chamber before batch processing begins. These components are prepared in advance to immediately capture any byproducts that escape during batch changes, reducing the need for frequent chamber openings and minimizing atmospheric contamination events.

Inventive Principle:
Principle #10Preliminary action

4Reliability

If cold traps are used to condense byproducts, then pump protection is improved, but device complexity and maintenance requirements worsen

Engineering Contradiction:
Improvepump protectionVSAvoidvacuum system complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent merges the byproduct removal function with existing chamber components rather than adding separate complex cold trap systems. Getter materials are integrated into the chamber structure, pump lines, and insulation layers, combining multiple functions into unified components and reducing overall system complexity.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design significantly reduces maintenance costs, prevents contamination, and ensures consistent product quality by keeping the chamber above the condensation temperature, minimizing byproduct condensation and maintaining dimensional integrity.

Implementation Method 1

Fluid inlet and outlet structures positioned to circulate heated thermal transfer fluid through the passages between the inner and outer walls maintain a controlled isothermal inner wall temperature above a condensation temperature

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Implementation Method 2

A layer of thermal insulation covers the outer wall. A layer of high temperature thermal insulation covers the inner wall.

Methodology Applied
Scientific EffectThermal insulation: Thermal Insulation

Implementation Method 3

Heating elements are positioned in the interior of the processing chamber to heat a substrate mounted in the chamber

Methodology Applied
Scientific EffectResistive heating: Joule Heating

Data Source

PatentUS10100409B2Isothermal warm wall CVD reactor
Publication Date: 2018.10.16 RTX CORP
  • US10100409B2 patent drawing
  • US10100409B2 patent drawing
  • US10100409B2 patent drawing

AI summary

A chemical vapor deposition (CVD) reactor includes a double wall vacuum processing chamber with an inner wall and an outer wall and fluid passages between the walls. A layer of thermal insulation covers the outer wall. A layer of high temperature thermal insulation covers the inner wall. Heating elements are positioned in the interior of the processing chamber to heat a substrate mounted in the chamber. A gas inlet structure is positioned through the inner and outer walls of the chamber and oriented to direct a flow of reactant gas against the substrate to form a CVD coating on the substrate. A gas outlet structure connected to a vacuum and effluent management system is positioned through the inner and outer walls of the chamber. Fluid inlet and outlet structures positioned to circulate heated thermal transfer fluid through the passages between the inner and outer walls maintain a controlled isothermal inner wall temperature above a condensation temperature of reactant gas and effluent reacted gas byproducts from condensing on the inner walls and insulation in the chamber.