L-glufosinate Salt Dispersion Process for Homogeneous Liquid Herbicides

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Solution Overview

Problem

The production of liquid herbicidal compositions of L-glufosinate salt is hindered by the formation of rock-solid lumps when it comes into contact with water, leading to reduced solubility, increased processing time, and equipment damage, making large-scale production cumbersome and costly.

Innovation Solution

A process involving the admixing of water with a dispersion comprising L-glufosinate salt and at least one organic solvent or liquid surfactant, without initial contact with water, to prevent rock-solid lump formation, thereby ensuring a homogeneous and efficient liquid herbicidal composition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If L-glufosinate salt is contacted with water directly, then it should dissolve readily, but it forms rock-solid lumps with low solubility

Engineering Contradiction:
Improvesolubility of L-glufosinate saltVSAvoidformation of rock-solid lumps
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent applies preliminary action by first forming a dispersion of L-glufosinate salt in an organic solvent before adding water. This preliminary dispersion step prevents the direct contact between L-glufosinate salt and water that causes rock-solid lump formation, thereby maintaining solubility while avoiding aggregation.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent uses an organic solvent as an intermediary substance between L-glufosinate salt and water. The organic solvent mediates the interaction by first dissolving the L-glufosinate salt to form a stable dispersion, which then mixes with water without forming rock-solid lumps, thus resolving the solubility-composition stability contradiction.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of manufacture

If L-glufosinate salt is mixed with water directly, then the composition can be prepared, but the process becomes cumbersome and time-consuming

Engineering Contradiction:
Improveease of producing liquid herbicidal compositionVSAvoidprocessing time
Core Design Contradiction:
Ease of manufactureVSLoss of time

Solution Approach 1:

The patent applies preliminary action by pre-forming a dispersion of L-glufosinate salt in an organic solvent before water addition. This preliminary step creates a stable intermediate formulation that mixes readily with water, significantly reducing the time and effort required for the overall composition preparation compared to direct mixing.

Inventive Principle:
Principle #10Preliminary action

3Ease of manufacture

If L-glufosinate salt is mixed with water directly, then the composition can be prepared, but equipment damage occurs and investment increases

Engineering Contradiction:
Improveease of producing liquid herbicidal compositionVSAvoidequipment damage
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent applies preliminary action by first creating a dispersion of L-glufosinate salt in an organic solvent. This preliminary dispersion step prevents the formation of rock-solid lumps during water addition, thereby eliminating the mechanical stress and damage to mixing equipment that would otherwise occur during direct water mixing.

Inventive Principle:
Principle #10Preliminary action

4Ease of manufacture

If L-glufosinate salt is mixed with water directly, then the composition can be prepared, but homogeneity is difficult to achieve

Engineering Contradiction:
Improveease of producing liquid herbicidal compositionVSAvoidhomogeneity of composition
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by first forming a uniform dispersion of L-glufosinate salt in an organic solvent. This preliminary dispersion ensures uniform distribution of the active ingredient before water addition, making it much easier to achieve a homogeneous final composition compared to direct water mixing where rock-solid lumps form and resist dissolution.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent uses an organic solvent as an intermediary to achieve better homogeneity. The organic solvent mediates the mixing process by first creating a uniform dispersion of L-glufosinate salt, which then integrates smoothly with water to produce a homogeneous liquid herbicidal composition without the aggregation problems of direct water mixing.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in a faster, more reliable, and cost-effective production of a homogeneous liquid herbicidal composition with improved bioavailability and efficiency, reducing processing time and equipment investment.

Implementation Method 1

forming a dispersion in the absence of water, wherein the dispersion comprises the L-glufosinate salt and at least one organic solvent or a liquid surfactant

Methodology Applied
Scientific EffectDispersion: Dispersion (of waves)

Implementation Method 2

admixing the dispersion with water to obtain a liquid herbicidal composition which is free from rock-solid lumps

Methodology Applied
Scientific EffectAdmixing:

Data Source

PatentUS20220279781A1Process for producing a liquid herbicidal composition
Publication Date: 2022.09.08 UPL LTD
  • US20220279781A1 patent drawing

AI summary

The present invention relates to an improved process for producing a liquid herbicidal composition of single isomer of glufosinate salt. The present invention also provides a method of controlling unwanted plants using said herbicidal compositions.