Large-Size Diamond MPCVD Device With Microwave-Shielded Windows

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Solution Overview

Problem

Existing MPCVD devices suffer from microwave leakage at the observation window and cavity door sealing, and lack the ability to monitor and optimize process parameters during diamond growth, leading to poor quality in mass-produced diamonds.

Innovation Solution

An MPCVD device with composite windows, pressure sensors, thickness and temperature measuring devices, and a plasma diagnostic device, coupled with an expert optimization system using artificial neural networks and genetic algorithms, to monitor and optimize diamond growth parameters in real time.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If an O-shaped sealing ring is arranged at the connection between the baseplate and the upper cover plate, then the sealing of the cavity door opening is improved, but microwave leakage occurs at the observation window and the ability to monitor process parameters is lost

Engineering Contradiction:
Improvesealing reliabilityVSAvoidmicrowave leakage
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent uses a composite window structure combining quartz material and microwave absorbing material. The quartz portion allows optical observation while the microwave absorbing material layer prevents microwave leakage, creating a composite solution that addresses both sealing reliability and microwave leakage issues simultaneously

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent introduces a microwave absorbing material as an intermediary substance between the sealing requirements and microwave transmission. This intermediary material absorbs microwaves while allowing the sealing structure to function, resolving the contradiction between sealing reliability and microwave leakage

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of operation

If process parameters are determined by worker experience, then the operation simplicity is maintained, but the diamond quality and consistency deteriorate

Engineering Contradiction:
Improveoperation simplicityVSAvoiddiamond quality consistency
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The patent implements a feedback mechanism where sensors continuously monitor process parameters (temperature, pressure, gas flow) and feed this information to the control system. The control system automatically adjusts parameters based on real-time feedback, ensuring consistent diamond quality while maintaining ease of operation through automated control

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The control system performs self-adjustment of process parameters based on pre-set optimization algorithms and real-time sensor data. The system automatically optimizes deposition conditions without requiring continuous manual intervention, achieving both high manufacturing precision and operational simplicity

Inventive Principle:
Principle #25Self-service

3Measurement precision

If multiple measurement and monitoring devices are added to the MPCVD device, then the ability to monitor and optimize process parameters is improved, but the device complexity increases

Engineering Contradiction:
Improveprocess parameter monitoring capabilityVSAvoiddevice structural complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent designs the upper cover plate with integrated multi-functional capabilities: it serves as a structural component, incorporates composite windows for observation and microwave shielding, and integrates multiple sensors (temperature, pressure, gas flow). This universal design approach allows one component to perform multiple functions, reducing overall device complexity while maintaining high measurement precision

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Prevents microwave leakage, ensures consistent diamond growth conditions, and enhances diamond quality by optimizing process parameters, resulting in high-quality large-size diamonds with low impurity content and high thermal conductivity.

Implementation Method 1

a microwave quartz window (5) arranged between the deposition platform and the baseplate, and the reaction cavity is isolated from the air outside by the microwave quartz window

Methodology Applied
Scientific EffectMicrowave radiation shielding: Microwave Radiation

Implementation Method 2

the connection between the baseplate and the upper cover plate is sealed by an O-shaped sealing ring assembly

Methodology Applied
Scientific EffectElastic sealing: Elasticity

Implementation Method 3

an exhaust hole that is connected with a vacuumizing device is arranged on the baseplate, for vacuumizing the reaction cavity to form a vacuum environment

Methodology Applied
Scientific EffectVacuum pumping: Vacuum

Implementation Method 4

the plasma diagnostic device is configured to measure the content of various carbon-containing groups on the growth surface of diamond

Methodology Applied
Scientific EffectPlasma spectroscopy: Plasma

Implementation Method 5

a thickness measuring device is configured to measure the growth thickness of the diamond in real time

Methodology Applied
Scientific EffectOptical measurement: Light

Implementation Method 6

the temperature measuring device is configured to detect the diamond temperature in real time

Methodology Applied
Scientific EffectThermal detection: Temperature Gradient

Implementation Method 7

the visual device is configured to detect surface defects and estimate temperature difference in real time

Methodology Applied
Scientific EffectOptical detection: Light

Data Source

PatentUS12448702B2Large-size diamond, MPCVD device and preparation method of large-size diamond
Publication Date: 2025.10.21 ZHENGZHOU RES INST FOR ABRASIVES & GRINDING CO LTD
  • US12448702B2 patent drawing
  • US12448702B2 patent drawing
  • US12448702B2 patent drawing

AI summary

MPCVD device comprises deposition platform, substrate platform, lifting platform, microwave quartz window, upper cover plate, baseplate, pressure sensors, composite windows, thickness measuring device, visual device, temperature measuring device, plasma diagnostic device, vacuum sealing ring and microwave shielding sealing ring. Reaction cavity is formed by upper cover plate and baseplate, and inlet hole is arranged on top of upper cover plate, while exhaust hole is arranged on baseplate; microwave quartz window is annular shaped and arranged between deposition platform and baseplate, and reaction cavity is isolated from air outside by microwave quartz window; lifting platform is provided with vacuum channel and cooling channel therein; vacuum cavity, which is communicated with vacuum channel, is formed by lower surface of substrate platform and upper surface of lifting platform; and pressure sensor for monitoring gas pressure is arranged in vacuum cavity.