Laser Ablation of Microparticles for Nanoparticle Production

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Solution Overview

Problem

Existing methods for producing three-dimensional nanostructured materials suffer from issues such as agglomeration, broad size distribution, low volume production, impurity, and environmental concerns, making it difficult to produce nanoparticles and nanostructured films on a practical scale for various applications.

Innovation Solution

The method involves generating aerosol gases of microparticles, subjecting them to laser ablation to produce nanoparticles, and then combining these nanoparticles to form composite, shelled, alloy, or compound nanoparticles, which are deposited onto substrates to create nanostructured films, allowing for controlled production of nanoparticles and films without agglomeration and surfactant requirements.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional methods (vacuum synthesis, gas-phase synthesis, condensed phase synthesis) are used to produce three-dimensional nanostructured materials, then nanoparticle films and structures can be formed, but the materials suffer from agglomeration, broad size distribution, low volume production, impurity, and environmental unfriendliness

Engineering Contradiction:
Improvenanoparticle size controlVSAvoidvolume production rate
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent replaces conventional mechanical and chemical synthesis methods with laser ablation, using electromagnetic energy to directly transform microparticles into nanoparticles. This substitution eliminates the need for chemical reagents, surfactants, and complex multi-step processes, achieving both high precision nanoparticle size control and high volume production rates simultaneously

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the fundamental parameter of particle size through controlled laser ablation duration and energy input. By adjusting laser parameters (pulse duration, intensity, wavelength) and processing conditions, the system can produce nanoparticles with narrow size distribution while maintaining high production rates, resolving the contradiction between precision and productivity

Inventive Principle:
Principle #35Parameter changes

2Reliability

If conventional synthesis methods are used, then nanoparticle films can be produced, but they require surfactants and produce impurities

Engineering Contradiction:
Improvenanoparticle composition purityVSAvoidprocess complexity
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent extracts and eliminates the need for surfactants, chemical reagents, and complex purification steps by using laser ablation in controlled atmospheres. The direct laser ablation process produces clean nanoparticles without contamination, and the system can operate in simple gas environments, greatly simplifying the manufacturing process while ensuring high purity

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent uses inert or controlled atmosphere environments during laser ablation to prevent oxidation and contamination of nanoparticles. This approach maintains nanoparticle purity without requiring complex chemical processing or purification steps, simplifying the overall manufacturing process while ensuring reliable composition

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

3Productivity

If existing manufacturing technologies are used, then nanoparticle production can be achieved, but only at scales that are difficult to scale for practical applications

Engineering Contradiction:
Improveproduction volumeVSAvoidnanoparticle size distribution
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent uses microparticles as pre-formed starting materials with controlled size and composition, then applies laser ablation to transform them into nanoparticles. This preliminary preparation of microparticles allows the system to maintain narrow size distribution while dramatically increasing production volume, as the microparticles serve as ready-to-process precursors that can be ablated at high rates

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent employs pulsed laser ablation with controlled repetition rates to produce nanoparticles continuously at high volumes. By optimizing the pulse frequency and energy delivery, the system maintains consistent nanoparticle size distribution while achieving high production rates suitable for practical applications

Inventive Principle:
Principle #19Periodic action

Data Source

PatentUS7527824B2Methods for producing coated nanoparticles from microparticles
Publication Date: 2009.05.05 INTELLECTUAL VENTURES HOLDING 40 LLC
  • US7527824B2 patent drawing
  • US7527824B2 patent drawing
  • US7527824B2 patent drawing

AI summary

A method for producing composite, shelled, alloy and compound nanoparticles as well as nanostructured films of composite, shelled, alloy and compound nanoparticles by using laser ablation of microparticles is disclosed.