Late GPAM Addition at Floc Junctions for Paper Dry Strength

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Solution Overview

Problem

Existing methods for enhancing dry strength in paper products often interfere with other additives, require excessive amounts of chemicals, and do not effectively utilize residence time, leading to suboptimal performance.

Innovation Solution

A method involving the addition of a cationic wet strength agent, flocculant, and glyoxalated polyacrylamide (GPAM) copolymer in the wet-end papermaking process, specifically at the last possible moment before entering the headbox, using acrylamide-acrylic acid copolymer intermediates with controlled molecular weights and residence times to target junction points between flocs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Duration of action of moving object

If glyoxalated polyacrylamide copolymer is added earlier in the process, then there is more time for the polymer to interact with fibers, but the polymer distributes uniformly throughout the sheet rather than concentrating at junction points

Engineering Contradiction:
Improveresidence timeVSAvoidpolymer distribution targeting
Core Design Contradiction:
Duration of action of moving objectVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by adding the GPAM copolymer at the very last moment before the slurry enters the headbox (within 18 seconds), after flocculation has already occurred. This timing allows the polymer to find and bind to junction points between flocs without having time to distribute uniformly throughout the entire sheet, thereby achieving precise spatial targeting through controlled timing of addition.

Inventive Principle:
Principle #10Preliminary action

2Strength

If vinylamine-containing polymers are used to enhance dry strength, then dry strength increases, but optical brightening agent performance is negatively affected

Engineering Contradiction:
Improvedry strengthVSAvoidoptical brightening agent performance
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The patent changes the chemical parameter of the polymer by using glyoxalated polyacrylamide copolymer instead of vinylamine-containing polymers. This parameter change maintains the dry strength enhancement function while eliminating the harmful interaction with optical brightening agents, as GPAM does not contain vinylamine groups that quench OBA fluorescence.

Inventive Principle:
Principle #35Parameter changes

3Strength

If more than optimal amounts of additives are used to enhance dry strength, then dry strength improves, but the process becomes difficult and cumbersome

Engineering Contradiction:
Improvedry strengthVSAvoidadditive application process
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent applies self-service by utilizing the natural flocculation process to create junction points that automatically serve as binding sites for the GPAM copolymer. The polymer adds itself to the most critical locations (junction points between flocs) without requiring complex application systems or excessive amounts of additive, as the floc structure guides the polymer to where it is most needed.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly increases dry strength in paper substrates by concentrating GPAM at floc junction points, resulting in superior dry strength properties compared to conventional methods.

Implementation Method 1

concentrating GPAM at floc junction points

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

adding a cationic wet strength agent and flocculant to a tissue or towel paper substrate

Methodology Applied
Scientific EffectFlocculation: Flocculation

Data Source

PatentEP3094779B1Wet end chemicals for dry end strength in paper
Publication Date: 2025.09.24 ECOLAB USA INC
  • EP3094779B1 patent drawingFigure 1
  • EP3094779B1 patent drawingFigure 2
  • EP3094779B1 patent drawingFigure 3

AI summary

The invention provides methods and compositions for increasing the dry strength of paper. The invention utilizes a tailored strength agent whose size and shape is tailored to fit into the junction points between flocs of a paper sheet. The strength agents is in contact with the slurry for just enough time to collect at the junction points but not so much that it can migrate away from there.