Layered Exhaust Gas Catalyst to Limit PGM Sintering and Migration

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing exhaust gas purification catalysts face degradation in performance due to sintering and migration of platinum group elements under high-temperature conditions, leading to reduced efficiency in purifying harmful components from engine exhaust.

Innovation Solution

A catalyst layer comprising a first layer with a specific composition of zirconium-cerium complex oxide and a second layer with aluminum oxide, each containing platinum group elements, is designed to maintain optimal performance by limiting sintering and migration, enhancing purification efficiency at low to medium temperatures.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If alumina and Zr-Ce-based complex oxide are contained in one layer, then alloying of platinum group elements can be suppressed, but sintering and migration of platinum group elements occur under high-temperature environment, leading to decreased exhaust gas purification performance

Engineering Contradiction:
Improvecomposition stability of catalyst layerVSAvoidexhaust gas purification performance
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The catalyst layer is divided into multiple sub-layers with distinct compositions. The first sub-layer contains alumina and Zr-Ce-based complex oxide with Pd, while the second sub-layer contains Rh supported on alumina. This segmentation prevents mixing of different platinum group elements and their supports, thereby suppressing sintering and migration that would occur if all components were in a single layer, while maintaining effective exhaust gas purification performance.

Inventive Principle:
Principle #1Segmentation

2Adaptability or versatility

If Zr-Ce-based complex oxide is used as support, then oxygen storage capacity is enhanced and operating window is expanded, but sintering of support materials occurs under high-temperature conditions, reducing catalyst durability

Engineering Contradiction:
Improveoperating window of catalystVSAvoidcatalyst durability
Core Design Contradiction:
Adaptability or versatilityVSDuration of action of stationary object

Solution Approach 1:

The catalyst layer is segmented into sub-layers where Zr-Ce-based complex oxide is specifically placed in the first sub-layer with Pd, separate from the Rh-containing second sub-layer. This segmentation prevents high-temperature sintering interactions between different supports and platinum group elements, maintaining the oxygen storage capacity and extended operating window while ensuring long-term catalyst durability through reduced thermal degradation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different regions (sub-layers) of the catalyst layer are assigned different compositions optimized for specific functions. The first sub-layer with Zr-Ce-based complex oxide and Pd is optimized for oxygen storage and low-temperature activity, while the second sub-layer with Rh on alumina is optimized for NOx reduction. This local quality differentiation prevents unwanted sintering interactions while maintaining overall catalyst performance and durability.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst layer configuration improves exhaust gas purification performance, particularly at low to medium temperatures, by suppressing sintering and migration of platinum group elements, thereby maintaining effective purification even after exposure to high temperatures.

Implementation Method 1

a three-way catalyst having a catalytic activity to oxidize HC and convert it to water and carbon dioxide, to oxidize CO and convert it to carbon dioxide as well as to reduce NOx and convert it to nitrogen

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

A Zr-Ce-based complex oxide has an oxygen storage capacity (OSC), and is advantageous in mitigating fluctuations in the oxygen concentration in the exhaust gas

Methodology Applied
Scientific EffectOxygen storage capacity: Absorption (physical)

Data Source

PatentEP4316651B1Exhaust gas purification catalyst
Publication Date: 2025.12.17 MITSUI MINING & SMELTING CO LTD
  • EP4316651B1 patent drawingFigure 1~2
  • EP4316651B1 patent drawingFigure 3
  • EP4316651B1 patent drawingFigure 4

AI summary

An object of the present invention is to provide an exhaust gas purification catalyst with improved exhaust gas purification performance, and in order to achieve such an object, the present invention provides an exhaust gas purification catalyst (1A) including a substrate (10) and a catalyst layer (20) provided on the substrate (10), wherein the catalyst layer (20) includes a first layer (21) containing Rh, and Pd and/or Pt, and a second layer (22) containing Rh, and Pd and/or Pt, wherein a total content of Zr and Ce in terms of oxide and a content of aluminum element in terms of oxide in the first layer (21) are 70% by mass or more and 15% by mass or less, respectively, based on a mass of the first layer (21), and wherein a content of aluminum element in terms of oxide and a total content of Zr and Ce in terms of oxide in the second layer (22) are 75% by mass or more and 15% by mass or less, respectively, based on a mass of the second layer (22).