Layered Lean Burn Catalyst for NOx and CO Purification

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Solution Overview

Problem

Conventional catalysts for lean-burn engines face challenges in effectively purifying NOx and CO over a wide temperature range, particularly at high temperatures, due to the deterioration of NOx storage capacity and reduced reductant availability.

Innovation Solution

A catalyst with an integrally structured support and a layered configuration, featuring a proton-substituted β-type zeolite and ceria-based oxide supporting rhodium in the upper layer, and a NOx storage component with an alkaline-earth metal compound and ceria-based oxide in the lower layer, along with platinum and palladium, to enhance NOx reduction and CO oxidation performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a conventional LNT catalyst is used to reductively remove NOx, then NOx purification is achieved, but the catalyst deteriorates at high temperatures and loses NOx storage capacity

Engineering Contradiction:
ImproveNOx purification performanceVSAvoidhigh temperature stability
Core Design Contradiction:
ReliabilityVSTemperature

Solution Approach 1:

The catalyst is divided into multiple functional layers: a first washcoat layer containing NOx storage material (barium oxide), a second washcoat layer containing hydrocarbon trap material (zeolite), and a nitrogen oxide conversion material layer. This segmentation allows each layer to perform its specific function optimally while protecting the overall system from high temperature deterioration.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The catalyst uses composite material structures including barium oxide-ceria composite in the NOx storage layer, and combines multiple materials (zeolite, precious metals, oxygen storage components) in different layers to create a synergistic system that maintains stability and performance at high temperatures.

Inventive Principle:
Principle #40Composite materials

2Productivity

If the amount of air is increased for lean burn operation, then fuel efficiency improves, but NOx becomes difficult to reductively remove due to insufficient reducing components

Engineering Contradiction:
Improvefuel efficiencyVSAvoidNOx reduction capability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The catalyst performs preliminary oxidation of CO and HC in the lean exhaust gas before the rich spike operation. The hydrocarbon trap material in the second washcoat layer stores reactive hydrocarbons that are then used during the rich spike for efficient NOx reduction, eliminating the need for external fuel injection.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The catalyst uses the exhaust gas components themselves (CO and HC) as reducing agents for NOx conversion. The system is self-sufficient by utilizing the fuel's own combustion products rather than requiring additional external reducing agents or complex control systems.

Inventive Principle:
Principle #25Self-service

3Reliability

If a three-way catalyst is used for stoichiometric operation, then CO and HC are easily oxidized, but the system cannot effectively purify NOx in lean burn conditions

Engineering Contradiction:
ImproveCO and HC oxidation performanceVSAvoidadaptability to lean burn operation
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The catalyst is designed with multi-functionality to handle both lean and rich conditions. The first washcoat layer stores NOx during lean operation, the second washcoat layer traps hydrocarbons, and the nitrogen oxide conversion material reduces NOx during rich spikes. This universal design allows a single catalyst to replace both TWC and LNT functions.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The catalyst operates by changing the air-fuel ratio parameter dynamically - maintaining lean operation for most of the time for efficiency, then briefly switching to rich conditions for NOx reduction. The catalyst materials are selected to respond to these parameter changes, with barium oxide storing NOx under lean conditions and releasing it under rich conditions.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst achieves high purification performance for NOx, CO, and HC across a wide temperature range, maintaining activity and stability even at high temperatures, thereby addressing the limitations of existing technologies.

Implementation Method 1

the upper layer containing at least a proton-substituted β-type zeolite and a ceria-based oxide supporting rhodium

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

the lower layer containing at least a NOx storage component and an inorganic oxide supporting platinum, wherein the NOx storage component contains an alkaline-earth metal compound and a ceria-based oxide

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 3

an inorganic oxide supporting platinum

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 4

hydrocarbon (HC) and carbon monoxide (CO), which are reducing components, can be oxidatively removed easily by excess oxygen

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentEP3476480B1Catalyst for lean burn
Publication Date: 2024.08.28 N E CHEMCAT
  • EP3476480B1 patent drawingFigure 1
  • EP3476480B1 patent drawingFigure 2~4

AI summary

The present invention relates to catalysts for lean burn and provides a catalyst for lean burn that is capable of purifying NOx sufficiently and that has a high ability to purify CO and HC over a wide temperature range from low to high temperatures. The present invention provides a catalyst for a lean-burn engine to purify exhaust gas, the catalyst including: an integrally structured support; and a catalyst layer containing a precious metal element, provided on the integrally structured support and having at least two layers that include an upper layer and a lower layer; wherein the upper layer of the catalyst layer contains at least a proton-substituted β-type zeolite and a ceria-based oxide supporting rhodium, and the lower layer of the catalyst layer contains at least a NOx storage component and platinum supported on an inorganic oxide.