LC-PUFA Vegetable Oil Oxidation Control via Seed Processing

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Solution Overview

Problem

Polyunsaturated fatty acids (PUFAs) with at least 20 carbon atoms (LC-PUFAs) are highly sensitive to oxidation, leading to oil of insufficient quality due to increased sensitivity with the number of double bonds and content, which existing methods fail to adequately address.

Innovation Solution

A process for obtaining a vegetable oil with LC-PUFAs, characterized by an anisidine value < 25, peroxide value < 10, triglyceride content > 90%, and an Oil Stability Index (OSI) > 5 hours at 80 °C, involving seed selection, drying at low temperatures, controlled storage, and extraction methods to enhance oil quality.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If the content of LC-PUFAs is increased in the oil, then the nutritional value and health benefits are improved, but the oxidation sensitivity and quality degradation increase

Engineering Contradiction:
ImproveLC-PUFA contentVSAvoidoxidation sensitivity
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent applies preliminary action by selecting and processing seeds before oil extraction to prevent oxidation during storage and processing. The seeds are dried at controlled temperatures and stored under specific conditions before extraction, preparing them in advance to minimize oxidation sensitivity in the final oil product.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent changes physical and chemical parameters of the oil through controlled processing. Specifically, the oil is processed to achieve specific anisidine values (<25), peroxide values (<10), and triglyceride content (>90%), transforming the oil's properties to reduce oxidation sensitivity while maintaining high LC-PUFA content.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If the number of double bonds in LC-PUFAs is increased, then the polyunsaturated fatty acid content is improved, but the oxidation sensitivity increases

Engineering Contradiction:
Improvepolyunsaturated fatty acid contentVSAvoidoxidation sensitivity
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent employs inert atmosphere principles by controlling the processing environment to minimize exposure to oxygen during oil extraction and storage. This creates a protective environment that reduces oxidation of the highly unsaturated fatty acids with multiple double bonds.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Solution Approach 2:

The patent uses intermediary substances and controlled processing conditions as mediators between the LC-PUFA-rich seeds and the final oil product. This includes using specific solvents, controlled temperatures, and processing intermediaries that protect the unsaturated fatty acids from direct oxidation during extraction.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If conventional oil extraction methods are used, then the extraction efficiency is maintained, but the oil quality and stability are insufficient

Engineering Contradiction:
Improveextraction efficiencyVSAvoidoil quality and stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent changes the parameters of the extraction process to achieve both efficiency and quality. Specific parameters include controlled temperature ranges, solvent selection, and processing speeds that are optimized to extract oil while maintaining anisidine value <25, peroxide value <10, and triglyceride content >90%.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent implements feedback mechanisms by monitoring oil quality parameters during the extraction process. The anisidine value, peroxide value, and triglyceride content are measured and used to adjust processing conditions in real-time to ensure the oil meets the required quality standards while maintaining extraction efficiency.

Inventive Principle:
Principle #23Feedback

Data Source

PatentEP2496091B1Vegetable oil comprising a polyunsaturated fatty acid having at least 20 carbon atoms
Publication Date: 2019.08.14 DSM IP ASSETS BV

AI summary

The present invention describes a vegetable oil comprising a polyunsatured fatty acid having at least 20 carbon atoms (LC-PUFA), which oil has (a) an anisidine value (An V) of less than 25; (b) a peroxide value (POV) of less than 10; (c) a triglyceride content of greater than 90%; and/or (d) an Oil Stability Index (OSI) of greater than 5 hours at 80 ºC.