LDPE Reactor Injector Geometry for Uniform Reactive Fluid Mixing

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Solution Overview

Problem

Existing reactor systems for high-pressure ethylene polymerization face issues with inadequate distribution of reactive fluids, leading to back mixing and material build-up, which affects the quality and consistency of polyethylene production, especially in severe production environments.

Innovation Solution

A reactor system with a device for injecting and mixing reactive fluids, featuring a cylindrically shaped injector part with a downstream nozzle and a fin-shaped support structure made from a single piece of metal, designed to minimize asymmetrical turbulence and prevent back mixing, with a tapered nozzle and wedge-shaped fronts to streamline fluid flow and reduce fouling.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If a conventional injector design is used to introduce reactive fluid into the reaction vessel, then the injection process is simple, but the reactive fluid is not sufficiently dispersed into ethylene gas causing local homopolymerization and gel-like materials

Engineering Contradiction:
Improvedispersion of reactive fluidVSAvoiduniformity of polymerization
Core Design Contradiction:
Quantity of substanceVSManufacturing precision

Solution Approach 1:

The injector design segments the reactive fluid injection into multiple stages: pre-mixing zone, main injection zone, and dispersion zone. The fluid is first pre-mixed with inert gas, then injected through multiple nozzle arrays arranged in segments along the reactor length, ensuring gradual dispersion rather than concentrated local injection

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

An intermediary inert gas (nitrogen or carbon dioxide) is introduced to carry and disperse the reactive fluid throughout the ethylene gas stream. This intermediary medium prevents direct contact between concentrated reactive fluid and ethylene, avoiding local homopolymerization while ensuring uniform distribution

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If high pressure conditions are used for LDPE production, then polymerization efficiency is improved, but material build-up and fouling occur in the reactor system

Engineering Contradiction:
Improvepolymerization efficiencyVSAvoidmaterial build-up and fouling
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The system performs preliminary action by pre-mixing the reactive fluid with inert gas and pre-heating the mixture before introduction to the high-pressure reaction zone. This preliminary preparation ensures controlled reaction initiation and prevents sudden localized reactions that cause material build-up

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The design converts the high-pressure condition, which normally causes fouling, into a benefit by using compressed inert gas to actively disperse reactive fluid. The high pressure that would concentrate reactants is instead used to drive the inert gas flow pattern that ensures uniform distribution, turning a harmful effect into a dispersing mechanism

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Reliability

If multiple separate components are used for the injector assembly, then manufacturing and assembly are flexible, but mechanical strength and reliability decrease under severe conditions

Engineering Contradiction:
Improvemechanical integrityVSAvoidinjector assembly structure
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The injector assembly merges multiple functional components (support structure, mounting brackets, nozzle holders, and injection manifolds) into a single integrated unit. This monolithic structure eliminates weak points at connection interfaces and ensures uniform stress distribution under high-pressure conditions, significantly improving mechanical reliability

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution ensures even distribution of the reactive fluid, reduces back mixing and fouling, and maintains mechanical integrity under harsh conditions, enabling efficient production of high-quality ethylene polymers at high pressures and temperatures.

Implementation Method 1

The device ensures even distribution of the injected fluid in a turbulent flow of the process fluid with a reduced back mixing

Methodology Applied
Scientific EffectTurbulence: Turbulence

Data Source

PatentEP3565659B1Device for injecting and mixing a reactive fluid in high pressure LDPE processes
Publication Date: 2022.01.26 SABIC GLOBAL TECHNOLOGIES BV
  • EP3565659B1 patent drawingFigure 1
  • EP3565659B1 patent drawingFigure 2
  • EP3565659B1 patent drawingFigure 3

AI summary

The invention relates to a device (100) for injecting and mixing a reactive fluid in a flow of a process fluid for the preparation of polyolefins, comprising: • an annular part (101) having an outer wall and an inner wall (102), wherein the annular part (101) is arranged for having a flow of the process fluid in a transport direction (F); • a support structure (103) connected to the inner wall (102) of the annular part (101); • an injector part (104) mounted on the support structure (103), wherein the injector part (104) is cylindrically shaped and wherein the cylindrical axis A-A' of the injector part is parallel with a central axis of the annular part and is in the central part of the annular part (101); wherein the injector part (104) comprises a nozzle (105) for injecting the reactive fluid, disposed at a downstream side of the injector part relative to the transport direction (F); • a supply channel (106) extending from the outer wall of the annular part (101) through the support structure (103) to the nozzle (105) of the injector part (104), and wherein the annular part (101), the support structure (103) and the injector part (104) are made from a single piece of metal.