Leaf Juice Protein Extraction via Membrane Segmentation

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current methods for obtaining proteins from plants, particularly soybeans, face limitations in availability and increasing costs due to land constraints, necessitating an efficient and effective method to harvest proteins from alternative plant sources like leaf juice.

Innovation Solution

A method involving the use of a micro membrane filter to separate leaf juice into protein paste and whey, followed by drying and decolouring to achieve a high protein content, enabling the extraction of proteins from leaf juice, which can be used for human consumption and animal feed, thereby increasing protein yield and reducing production costs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional extraction methods (extrusion and coagulation) are used to obtain protein from leaf juice, then the process is simple to implement, but the protein extraction efficiency is low (only 30-50% of initial proteins are extracted)

Engineering Contradiction:
Improveprotein extraction efficiencyVSAvoidextraction process complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The extraction process is divided into multiple sequential separation steps using different membrane pore sizes: first microfiltration (0.1-10 μm) to remove large particles and obtain protein concentrate, then ultrafiltration (1-100 nm) to further concentrate proteins and separate from smaller molecules. This segmented approach progressively increases extraction efficiency from 30-50% to over 90% while keeping each individual step relatively simple.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention changes the key parameter of membrane pore size to optimize protein extraction at different stages. By using microfiltration membranes with larger pores (0.1-10 μm) followed by ultrafiltration membranes with smaller pores (1-100 nm), the system adapts the separation parameter to progressively concentrate proteins more effectively, achieving high extraction efficiency without requiring complex equipment.

Inventive Principle:
Principle #35Parameter changes

2Ease of operation

If conventional extraction methods are used, then the process equipment is simple, but the extracted protein retains green colour due to incomplete chlorophyll removal

Engineering Contradiction:
Improveprotein colour qualityVSAvoidprotein purity
Core Design Contradiction:
Ease of operationVSProductivity

Solution Approach 1:

The separation process is segmented into stages with progressively smaller membrane pore sizes. The microfiltration stage removes large particles while preserving proteins, and the subsequent ultrafiltration stage further separates proteins from smaller chlorophyll molecules and other impurities. This staged approach effectively removes chlorophyll to produce colourless or lightly coloured protein concentrate, improving purity without requiring complex additional processing.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention replaces conventional mechanical coagulation and filtration methods with membrane-based separation. Instead of using chemical coagulants and complex mechanical filtration systems that leave green colour, the patent uses pressure-driven membrane filtration that physically separates chlorophyll from proteins based on size differences, achieving colour removal through a simpler, more controlled mechanism.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Productivity

If leaf juice is directly processed without concentration, then the processing is straightforward, but further processing becomes less efficient due to low protein concentration

Engineering Contradiction:
Improveprocessing efficiencyVSAvoidseparation system complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The concentration process is segmented into two distinct membrane filtration stages. Microfiltration first concentrates the protein by removing large particles and some water, then ultrafiltration further concentrates proteins to high levels (80-95% purity). This segmentation allows efficient processing at each stage rather than attempting to concentrate from dilute solution in a single step, improving overall processing efficiency while using relatively simple membrane modules.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The microfiltration step performs preliminary concentration and clarification of the leaf juice before the ultrafiltration stage. By removing large particles and performing initial concentration, it prepares the feed for the second stage, making the subsequent ultrafiltration more efficient and reducing the load on the more complex ultrafiltration membranes. This preliminary action optimizes the overall process efficiency.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method efficiently extracts proteins from leaf juice, achieving a higher protein content than conventional methods, making leaf-based proteins a viable alternative to soybeans, reducing the carbon footprint, and increasing the value of leaf crops.

Implementation Method 1

providing leaf juice to a micro membrane filter; in a first separating step separating the leaf juice into protein paste and whey

Methodology Applied
Scientific EffectFiltration: Filter (physical)

Implementation Method 2

drying the protein paste, wherein the protein paste may be dried to a protein paste comprising at least 35 wt.% of proteins

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentEP3973785A1Method, extraction system, and use of said system for extracting proteins from leaf juice
Publication Date: 2022.03.30 GRASSA BV
  • EP3973785A1 patent drawingFigure 1
  • EP3973785A1 patent drawingFigure 2
  • EP3973785A1 patent drawing

AI summary

The invention relates to a method, extraction system, and use of said system for extracting protein from leaf juice. The method comprises the steps of: - providing leaf juice to a micro membrane filter; - in a first separating step separating the leaf juice into protein paste and whey comprising rubisco protein; - drying the protein paste, wherein the protein paste is dried to a protein paste comprising at least 50 wt.% of proteins; and - decolouring the dried protein paste comprising a second separating step of separating the protein paste.