LED Excitation Source for AlphaScreen Optical Measurement

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Solution Overview

Problem

Current optical measurement technologies using laser diodes for excitation in AlphaScreen and similar chemiluminescence assays face challenges such as high power consumption, heat generation, complexity, and reduced sample reusability due to temperature sensitivity, leading to limited measurement capabilities and increased costs.

Innovation Solution

Employing a Light-Emitting Diode (LED) as the excitation light source, which provides consistent optical power without temperature-related issues, allowing for multiple measurements over time and reducing background interference through confocal optics and calibrated LED emission, enabling more sensitive and reliable detection of chemiluminescence signals.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Power

If a laser diode is used as the excitation light source, then high power density and uniform wavelength are achieved, but heat generation and temperature sensitivity increase, requiring active cooling and reducing sample reusability

Engineering Contradiction:
Improvepower densityVSAvoidtemperature stability
Core Design Contradiction:
PowerVSTemperature

Solution Approach 1:

The patent extracts the harmful thermal effects from the excitation light source by replacing the laser diode with an LED. The LED provides sufficient excitation power without generating the same level of heat as the laser diode, eliminating the need for active cooling systems and Peltier coolers while maintaining temperature stability.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent adopts a simpler, more robust LED light source that does not require complex cooling infrastructure. While LEDs have shorter operational lifetimes compared to laser diodes, they eliminate the need for expensive cooling systems and reduce overall system complexity, making the instrument more cost-effective and easier to maintain.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Power

If a laser diode is used as the excitation light source, then high excitation energy is achieved, but device complexity and cost increase due to required cooling systems

Engineering Contradiction:
Improveexcitation energyVSAvoidsystem complexity
Core Design Contradiction:
PowerVSDevice complexity

Solution Approach 1:

The patent removes the complex cooling subsystems (Peltier coolers, temperature control circuits, and associated hardware) by replacing the laser diode with an LED. The LED provides adequate excitation energy for AlphaScreen measurements without generating sufficient heat to require active cooling, thereby simplifying the overall instrument architecture.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent employs a simpler, more affordable LED light source that eliminates the need for expensive cooling infrastructure. Although LEDs may have shorter operational lifetimes, they significantly reduce system complexity and cost by removing temperature control mechanisms, making the instrument more accessible and easier to maintain.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Power

If a laser diode is used for sample excitation, then high power density is achieved, but sample reusability is reduced due to photobleaching and signal degradation

Engineering Contradiction:
Improvepower densityVSAvoidsample reusability
Core Design Contradiction:
PowerVSReliability

Solution Approach 1:

The patent changes the key parameter of the light source from high power density (laser diode) to lower power density with sufficient total energy (LED). This parameter change reduces the photobleaching effect on the sample while still providing adequate excitation for the AlphaScreen reaction, allowing multiple measurements to be performed on the same sample over time.

Inventive Principle:
Principle #35Parameter changes

4Measurement precision

If conventional fluorescence measurement is performed, then emission light detection is achieved, but background fluorescence interference reduces measurement sensitivity

Engineering Contradiction:
Improvedetection sensitivityVSAvoidbackground fluorescence
Core Design Contradiction:
Measurement precisionVSObject-generated harmful factors

Solution Approach 1:

The patent employs time-resolved measurement where the LED excitation source is pulsed and the emission signal is detected after a delay period. This periodic action allows the short-lived background fluorescence to decay before measurement, while the longer-lived chemiluminescent signal from the AlphaScreen reaction is measured, thereby improving signal-to-noise ratio and detection sensitivity.

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The LED-based system enhances measurement sensitivity, allows for multiple sample excitations without signal degradation, and reduces background noise, enabling reliable detection of lower analyte concentrations and kinetic studies with improved accuracy and cost-effectiveness.

Implementation Method 1

The liquid sample in the sample well is exposed to excitation light at a first wavelength from an LED excitation light source, which excitation light generates a collection of singlet state oxygen molecules from the liquid sample

Methodology Applied
Scientific EffectPhotoluminescence: Photoluminescence

Implementation Method 2

said singlet state oxygen molecules reacting with acceptor molecules in the liquid sample causing said acceptor molecules to emit chemiluminescence emission light at a second wavelength

Methodology Applied
Scientific EffectChemiluminescence: Chemiluminescence

Data Source

PatentEP3189325B1Method and apparatus for optical measurement of a liquid sample
Publication Date: 2022.02.09 LIFE TECH HLDG PTE LTD
  • EP3189325B1 patent drawingFigure 1
  • EP3189325B1 patent drawingFigure 2A~2B
  • EP3189325B1 patent drawingFigure 3

AI summary

A method and an apparatus for optical measurement of a liquid sample (2) placed in a sample well (3) where the sample in the sample well is exposed to excitation light (7) at first wavelength from an excitation light source (4), which excitation light generates a collection of singlet state oxygen molecules from donor molecules in the liquid sample, said singlet state oxygen molecules reacting with acceptor molecules in the liquid sample causing said acceptor molecules to emit chemiluminescence emission light (11) at second wavelength, which second wavelength is shorter than said first wavelength, and where the emission light produced by the excitation light is measured with a detector, characterized in that the excitation light source is a LED (4).