Li-Fe-Mn-Ti Phosphate Cathode Composition for Low-Temperature Capacity

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Solution Overview

Problem

Existing rechargeable lithium batteries face challenges in achieving high energy density, high operating voltage, and improved low-temperature characteristics.

Innovation Solution

A positive electrode active material comprising a compound represented by Formula Li a Fe x Mn y Ti z PO 4-b, with specific stoichiometric ranges for a, x, y, and z, is used, along with a conductive material and binder, to form a positive electrode layer that enhances conductivity and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If high capacity positive electrode materials are used to increase energy density, then the battery capacity increases, but the operating voltage decreases and low-temperature characteristics deteriorate

Engineering Contradiction:
Improvebattery capacityVSAvoidlow-temperature characteristics
Core Design Contradiction:
Quantity of substanceVSTemperature

Solution Approach 1:

The patent applies parameter changes by precisely controlling the stoichiometric ratios of elements in the Li-Fe-Mn-Ti-P compound system. By adjusting the content ranges of Li (0.95-1.05), Fe (0.70-0.85), Mn (0.10-0.25), and Ti (0.02-0.08), the invention optimizes the balance between capacity and low-temperature performance without changing the fundamental material structure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by creating a multi-element doped lithium iron phosphate compound (Li-Fe-Mn-Ti-P) that combines the advantages of different elements. Fe provides high capacity, Mn improves voltage and low-temperature characteristics, Ti enhances structural stability, and P maintains the phosphate framework, achieving synergistic effects that resolve the contradiction between capacity and temperature performance.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If high capacity positive electrode materials are used to increase energy density, then the battery capacity increases, but the operating voltage decreases

Engineering Contradiction:
Improvebattery capacityVSAvoidoperating voltage
Core Design Contradiction:
Quantity of substanceVSPower

Solution Approach 1:

The patent applies parameter changes by optimizing the stoichiometric composition parameters of the Li-Fe-Mn-Ti-P compound. By controlling Fe content at 0.70-0.85 and Mn content at 0.10-0.25, the invention achieves a balance where Fe provides high capacity while Mn maintains operating voltage above 3.3V through its electrochemical properties.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by formulating a Li-Fe-Mn-Ti-P quaternary doped compound where Fe and Mn work synergistically. Fe contributes to high capacity through multiple electron transitions, while Mn elevates the operating voltage to 3.3V or higher, resolving the contradiction between capacity and voltage.

Inventive Principle:
Principle #40Composite materials

3Ease of manufacture

If conventional positive electrode materials are used, then the manufacturing process is simple, but the energy density and conductivity are insufficient

Engineering Contradiction:
Improvemanufacturing process simplicityVSAvoidenergy density
Core Design Contradiction:
Ease of manufactureVSQuantity of substance

Solution Approach 1:

The patent applies parameter changes by modifying the compositional parameters of conventional lithium iron phosphate through multi-element doping. By introducing controlled amounts of Mn (0.10-0.25) and Ti (0.02-0.08) into the LiFePO4 structure, the invention enhances energy density and conductivity while maintaining a relatively simple solid-state reaction manufacturing process.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by creating a Li-Fe-Mn-Ti-P quaternary doped compound that integrates multiple functional elements into a single phase material. This composite approach improves energy density and electrical conductivity through synergistic effects while keeping the manufacturing process feasible through conventional ceramic processing techniques.

Inventive Principle:
Principle #40Composite materials

4Quantity of substance

If high capacity positive electrode materials are used, then the battery capacity increases, but manganese dissolution increases reducing reliability

Engineering Contradiction:
Improvebattery capacityVSAvoidmanganese dissolution resistance
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent applies parameter changes by optimizing the Mn content parameter within a specific range (0.10-0.25) and introducing Ti doping (0.02-0.08). This controlled parameter adjustment prevents excessive Mn dissolution by maintaining Mn content at moderate levels while Ti stabilizes the crystal structure, preventing Mn leaching even at high capacities.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by creating a Li-Fe-Mn-Ti-P quaternary doped compound where Ti acts as a structural stabilizer. The Ti elements reinforce the phosphate framework, preventing Mn dissolution into the electrolyte, while Fe and Mn provide high capacity. This composite structure resolves the contradiction between capacity and reliability.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution results in a rechargeable lithium battery with improved energy density, operating voltage, and low-temperature performance, while minimizing manganese dissolution and facilitating electrode processing.

Implementation Method 1

a positive electrode and a negative electrode (each containing an active material capable of intercalation and deintercalation of lithium ions)

Methodology Applied
Scientific EffectIntercalation and deintercalation of lithium ions:

Implementation Method 2

Electrical energy is produced by oxidation and reduction reactions when the lithium ions are intercalated into and deintercalated from the positive electrode and the negative electrode

Methodology Applied
Scientific EffectOxidation and reduction reactions: Redox Reactions

Data Source

PatentEP4641689A1Positive electrode active material for rechargeable lithium battery, positive electrode containing the same, and rechargeable lithium battery including the same
Publication Date: 2025.10.29 SAMSUNG SDI CO LTD
  • EP4641689A1 patent drawingFigure 1
  • EP4641689A1 patent drawingFigure 2
  • EP4641689A1 patent drawingFigure 3

AI summary

A positive electrode active material for a rechargeable lithium battery, a positive electrode containing the same, and a rechargeable lithium battery including the same are disclosed. A positive electrode active material includes a first particle containing a compound represented by Formula 1 and having a first average particle diameter:         Formula 1     LiaFexMnyTizPO4-b where, in Formula 1, 0.8≤a≤1.2, 0.79≤x≤0.9, 0.1≤y≤0.2, 0.001≤z≤0.05, 0≤b≤0.05, and 0.99≤x + y +z≤1.01.